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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘代甲苯
合成路线
（共 446 条）
615-37-2
2-碘代甲苯
+
75-86-5
丙酮氰醇
→
反应条件
529-19-1
邻甲基苯腈
反应条件
1: 1-iodo-2-methylbenzene With copper(l) iodide; 1,10-phenanthroline; potassium iodide in N,N-dimethyl-formamide T=110°C; 6 h; 2: 2-hydroxy-2-methyl-propionitrile With tributyl-amine in N,N-dimethyl-formamide T=110°C; 48 h;
参考文献
Cristau, Henri-Jean; Ouali, Armelle; Spindler, Jean-Francis; Taillefer, Marc
Chemistry - A European Journal, 2005 , vol. 11, # 8 p. 2483 - 2492
615-37-2
2-碘代甲苯
+
77287-34-4
甲亚胺酸
→
反应条件
529-19-1
邻甲基苯腈
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trichlorophosphate T=140°C; 48 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Wagh, Yogesh S.; Tambade, Pawan J.; Bhatte, Kushal D.; Bhanage, Bhalchandra M.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 781 - 787
615-37-2
2-碘代甲苯
+
151-50-8
氰化钾
→
反应条件
529-19-1
邻甲基苯腈
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene in various solvent(s) T=60°C; 4 h;
参考文献
Takagi, Kentaro; Sasaki, Ken; Sakakibara, Yasumasa
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1118 - 1121
615-37-2
2-碘代甲苯
→
反应条件
529-19-1
邻甲基苯腈
反应条件
copper(l) iodide; 1,10-phenanthroline in N,N-dimethyl acetamide T=140°C; 24 h;
参考文献
Zhu, Yi-Zhong; Cai, Chun
Journal of Chemical Research, 2007 , # 8 p. 484 - 485
615-37-2
2-碘代甲苯
+
109-77-3
丙二腈
→
反应条件
529-19-1
邻甲基苯腈
反应条件
potassium fluoride; 1,10-phenanthroline; copper diacetate; sodium t-butanolate in N,N-dimethyl-formamide T=120°C; 18 h;
参考文献
Jiang, Zhaoqiong; Huang, Qing; Chen, Si; Long, Lasheng; Zhou, Xiangge
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 589 - 592
615-37-2
2-碘代甲苯
+
75-05-8
乙腈
→
反应条件
529-19-1
邻甲基苯腈
反应条件
copper diacetate; triphenyl-phosphine oxide; silver(l) oxide T=125°C; 72 h;
参考文献
Song, Ren-Jie; Wu, Ji-Cheng; Liu, Yu; Deng, Guo-Bo; Wu, Cui-Yan; Wei, Wen-Ting; Li, Jin-Heng
Synlett, 2012 , vol. 23, # 17 p. 2491 - 2496,6
615-37-2
2-碘代甲苯
+
7677-24-9
三甲基氰硅烷
→
反应条件
529-19-1
邻甲基苯腈
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine 0.5 h; Heating;
参考文献
Chatani, Naoto; Hanafusa, Terukiyo
Journal of Organic Chemistry, 1986 , vol. 51, # 24 p. 4714 - 4716
→
反应条件
529-19-1
邻甲基苯腈
反应条件
tetrabutylammomium bromide; copper (II) acetate monohydrate in water T=180°C; 22 h;
参考文献
Ren, Yunlai; Zhao, Shuang; Tian, Xinzhe; Liu, Zhifei; Wang, Jianji; Yin, Weiping
Letters in Organic Chemistry, 2009 , vol. 6, # 7 p. 564 - 567
615-37-2
2-碘代甲苯
→
反应条件
7651-86-7
4-羟基菲
反应条件
1.1: 78 percent / Pd(PPh3)4; aq. Na2CO3 / 1,2-dimethoxy-ethane / Heating 2.1: 92 percent / LDA / tetrahydrofuran / 20 °C 3.1: n-BuLi / tetrahydrofuran; hexane / 0.08 h / 0 °C 3.2: 71 percent / tetrahydrofuran / -40 - 20 °C 4.1: 93 percent / aq. HCO2H; Pd(OAc)2; Ph3P / dimethylformamide / 60 - 70 °C 5.1: 91 percent / BBr3 / CH2Cl2 / -78 - 20 °C View Scheme
参考文献
Fu, Jian-Min; Snieckus, Victor
Canadian Journal of Chemistry, 2000 , vol. 78, # 6 p. 905 - 919
615-37-2
2-碘代甲苯
→
反应条件
7745-92-8
2-碘-4-硝基甲苯
+
5326-38-5
2-碘-5-硝基甲苯
+
6277-17-4
2-碘-3-硝基甲苯
反应条件
nitric acid; trifluoroacetic anhydride in acetic anhydride 0.333333 h; Ambient temperature;
参考文献
Bushnell, Gordon W.; Fischer, Alfred; Ibrahim, Prabha N.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1281 - 1286
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