反应条件
1: tetrakis(triphenylphosphine) palladium(0); triethylamine; copper(l) iodide / toluene / 4 h / 20 °C / |Inert atmosphere; |Schlenk technique 2: potassium carbonate / methanol / 3 h / 20 °C 3: tetrakis(triphenylphosphine) palladium(0); hydrogenchloride / tetrahydrofuran; water / 168 h / 45 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Superchi, Stefano; Sotomayor, Nuria; Miao, Guobin; Joseph, Babu; Snieckus, Victor
Tetrahedron Letters, 1996 , vol. 37, # 34 p. 6057 - 6060