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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘代甲苯
合成路线
（共 446 条）
615-37-2
2-碘代甲苯
+
67-68-5
二甲基亚砜
→
反应条件
14092-00-3
2-甲苄基硫醇
反应条件
ZnF2; copper(I) bromide T=150°C; 36 h; Sealed tubeUnder air;
参考文献
Luo, Fang; Pan, Changduo; Li, Liping; Chen, Fan; Cheng, Jiang
Chemical Communications, 2011 , vol. 47, # 18 p. 5304 - 5306
615-37-2
2-碘代甲苯
+
74-88-4
甲基碘
→
反应条件
14092-00-3
2-甲苄基硫醇
反应条件
1: 1-iodo-2-methylbenzene With potassium tert-butylate; thiolacetic acid potassium salt in dimethyl sulfoxide 3 h; Irradiation; 2: methyl iodide in water; dimethyl sulfoxide
参考文献
Schmidt, Luciana C.; Rey, Valentina; Penenory, Alicia B.
European Journal of Organic Chemistry, 2006 , # 9 p. 2210 - 2214
615-37-2
2-碘代甲苯
+
74-88-4
甲基碘
→
反应条件
4537-05-7
+
14092-00-3
2-甲苄基硫醇
反应条件
1: 1-iodo-2-methylbenzene With potassium tert-butylate; thiolacetic acid potassium salt in dimethyl sulfoxide 3 h; Irradiation; 2: methyl iodide in water; dimethyl sulfoxide
参考文献
Schmidt, Luciana C.; Rey, Valentina; Penenory, Alicia B.
European Journal of Organic Chemistry, 2006 , # 9 p. 2210 - 2214
615-37-2
2-碘代甲苯
→
反应条件
137622-07-2
反应条件
anilinium hypophosphorous salt; triethylamine; tetrakis(triphenylphosphine) palladium(0) in acetonitrile 2 h; Heating;
参考文献
Montchamp; Dumond
Journal of the American Chemical Society, 2001 , vol. 123, # 3 p. 510 - 511
615-37-2
2-碘代甲苯
+
74-88-4
甲基碘
→
反应条件
反应条件
1: 1-iodo-2-methylbenzene With potassium tert-butylate; KSeCN in dimethyl sulfoxide 3 h; Inert atmosphereIrradiation; 2: methyl iodide in dimethyl sulfoxide Inert atmosphere;
参考文献
Bouchet, Lydia M.; Penenory, Alicia B.; Argueello, Juan E.
Tetrahedron Letters, 2011 , vol. 52, # 9 p. 969 - 972
615-37-2
2-碘代甲苯
+
122-52-1
亚磷酸三乙酯
→
反应条件
15286-11-0
二乙基(2-甲基苯基)膦酸酯
反应条件
48 h; Irradiation;
参考文献
Obrycki,R.; Griffin,C.E.
Journal of Organic Chemistry, 1968 , vol. 33, p. 632 - 636
615-37-2
2-碘代甲苯
+
64723-95-1
+
29800-93-9
→
反应条件
15286-11-0
二乙基(2-甲基苯基)膦酸酯
反应条件
in ammonia T=-33°C; Irradiationcompetitive reaction, at known concentrations; relative rate constants, half life; Product distribution;
参考文献
Bunnett, Joseph F.; Mitchel, Eric; Galli, Carlo
Tetrahedron, 1985 , vol. 41, # 19 p. 4119 - 4132
615-37-2
2-碘代甲苯
→
反应条件
167708-86-3
反应条件
1: NBS; benzoyl peroxide / CCl4 / 12 h / Heating 2: dimethylformamide / 12 h / 80 °C View Scheme
参考文献
Orita, Akihiro; Miyamoto, Kazuhiko; Nakashima, Mikio; Ye, Fangguo; Otera, Junzo
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 7 p. 767 - 776
615-37-2
2-碘代甲苯
→
反应条件
17064-20-9
反应条件
bis-triphenylphosphine-palladium(II) chloride; n-butyllithium in tetrahydrofuran; diethyl ether; hexane 2 h; Heating;
参考文献
Anderson, Benjamin A.; Harn, Nancy K.
Synthesis, 1996 , # 5 p. 583 - 585
615-37-2
2-碘代甲苯
→
反应条件
16419-60-6
反应条件
1: With tBuCH2CH2B(H)NiPr2; triethylamine; triphenylphosphine; palladium dichloride in tetrahydrofuran T=65°C; Alcaraz-Vaultier borylation; 12 h; Inert atmosphere; 2: With methanol in tetrahydrofuran T=0°C; Inert atmosphere; Further stages;
参考文献
Haddenham, Dustin; Bailey, Christopher L.; Vu, Chau; Nepomuceno, Gabby; Eagon, Scott; Pasumansky, Lubov; Singaram, Bakthan
Tetrahedron, 2011 , vol. 67, # 3 p. 576 - 583
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