您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1,2-二碘苯
合成路线
（共 182 条）
615-42-9
1,2-二碘苯
+
201230-82-2
+
104-94-9
对甲氧基苯胺
→
反应条件
2142-04-3
2-(4-甲氧基苯基)异吲哚-1,3-二酮
反应条件
1,4-diaza-bicyclo[2.2.2]octane; palladium 10 on activated carbon in toluene T=120°C; P=4654.46 Torr; 2 h; Autoclave;
参考文献
Khedkar, Mayur V.; Khan, Shoeb R.; Sawant, Dinesh N.; Bagal, Dattatraya B.; Bhanage, Bhalchandra M.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3415 - 3422
615-42-9
1,2-二碘苯
+
201230-82-2
+
106-49-0
对甲苯胺
→
反应条件
2142-03-2
反应条件
1,4-diaza-bicyclo[2.2.2]octane; palladium 10 on activated carbon in toluene T=120°C; P=4654.46 Torr; 2 h; Autoclave;
参考文献
Khedkar, Mayur V.; Khan, Shoeb R.; Sawant, Dinesh N.; Bagal, Dattatraya B.; Bhanage, Bhalchandra M.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3415 - 3422
615-42-9
1,2-二碘苯
+
3085-54-9
4-甲酰苯胺
→
反应条件
2142-03-2
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trichlorophosphate T=140°C; 20 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Wagh, Yogesh S.; Bhatte, Kushal D.; Bhanage, Bhalchandra M.
European Journal of Organic Chemistry, 2011 , # 33 p. 6719 - 6724
615-42-9
1,2-二碘苯
+
106-95-6
3-溴丙烯
→
反应条件
74190-01-5
反应条件
1: 1,2-diiodobenzene With diethylzinc; 1-tert-butyl-4,4,4-tris(dimethylamino)-2,2-bis[tris(dimethylamino)-phosphoranylidenamino]-2Λ54Λ5-catenadi(phosphazene) in hexane; N,N-dimethyl acetamide T=20°C; 24 h; Inert atmosphere; 2: allyl bromide in hexane; N,N-dimethyl acetamide T=20°C; 24 h; Inert atmosphere;
参考文献
Naka, Hiroshi; Ito, Keisuke; Ueno, Masahiro; Kobayashi, Koji; Kondo, Yoshinori
New Journal of Chemistry, 2010 , vol. 34, # 8 p. 1700 - 1706
615-42-9
1,2-二碘苯
+
595585-52-7
→
反应条件
66291-33-6
反应条件
1: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide in tetrahydrofuran Suzuki cross-coupling reaction; 12 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene T=20°C; 0.5 h;
参考文献
Hilt, Gerhard; Hess, Wilfried; Schmidt, Frank
European Journal of Organic Chemistry, 2005 , # 12 p. 2526 - 2533
615-42-9
1,2-二碘苯
→
反应条件
68427-26-9
反应条件
1: 56 percent / Et3N, CuI / (Ph3P)2PdCl2 / tetrahydrofuran / Ambient temperature 2: 94 percent / Et3N, CuI / (Ph3P)2PdCl2 / tetrahydrofuran / Ambient temperature 3: 89 percent / PCC / CH2Cl2 / 8 h 4: 84 percent / diethyl ether / 0.5 h / Ambient temperature 5: 97 percent / K2CO3 / methanol / 0.5 h / Ambient temperature 6: 90 percent / PCC / CH2Cl2 / 2 h 7: 79 percent / 1,4-cyclohexadiene / chlorobenzene / 8 h / 190 °C View Scheme
参考文献
Grissom, Janet Wisniewski; Klingberg, Detlef; Meyenburg, Sabine; Stallman, Brenda L.
Journal of Organic Chemistry, 1994 , vol. 59, # 25 p. 7876 - 7888
615-42-9
1,2-二碘苯
→
反应条件
80510-04-9
反应条件
暂无反应条件数据
参考文献
Cytec Technology Corp.
Patent: US6563005 B1, 2003 ;
615-42-9
1,2-二碘苯
→
反应条件
823226-92-2
反应条件
1: n-BuNH2; CuI / Pd(PPh3)4 / diethyl ether 2: 86 percent / potassium carbonate / methanol 3: 86 percent / n-BuNH2; CuI / Pd(PPh3)4 / diethyl ether / 6 h View Scheme
参考文献
Lin, Chi-Fong; Lo, Yu-Hsiang; Hsieh, Ming-Chu; Chen, Yi-Hua; Wang, Jeh-Jeng; Wu, Ming-Jung
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 10 p. 3565 - 3575
615-42-9
1,2-二碘苯
+
874-90-8
→
反应条件
838-34-6
反应条件
copper(l) iodide; acetaldehyde oxime; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene T=120°C; 15 h; Inert atmosphereSchlenk technique;
参考文献
Zhang, Dong-Xue; Xiang, Shi-Kai; Hu, Hao; Tan, Wen; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Tetrahedron, 2013 , vol. 69, # 47 p. 10022 - 10029
615-42-9
1,2-二碘苯
→
反应条件
883-33-0
反应条件
1: (i) Cu, (ii) KOH 2: SOCl2 3: (heating) View Scheme
参考文献
Staab,A. et al.
Chemische Berichte, 1972 , vol. 105, p. 2290 - 2309
首页
上一页
1
...
12
13
14
15
16
17
18
19
下一页
末页
到第
页
确定
