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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘苯胺
合成路线
（共 712 条）
615-43-0
2-碘苯胺
→
反应条件
242792-95-6
7-苯基靛红
反应条件
1: 83 percent / hydroxylamine hydrochloride; sodium sulfate; aq. HCl / 55 °C 2: 80 percent / conc. sulfuric acid / 55 - 80 °C 3: 74 percent / aq. sodium bicarbonate / tetrakis[triphenylphosphine]palladium / 1,2-dimethoxy-ethane / Heating View Scheme
参考文献
Lisowski, Vincent; Robba, Max; Rault, Sylvain
Journal of Organic Chemistry, 2000 , vol. 65, # 13 p. 4193 - 4194
75-15-0
二硫化碳
+
107-03-9
丙硫醇
+
615-43-0
2-碘苯胺
→
反应条件
27410-43-1
2-(丙基硫基)-1,3-苯并噻唑
反应条件
1: carbon disulfide; propane-1-thiol With potassium carbonate in N,N-dimethyl-formamide T=20°C; 1 h; 2: 2-iodo aniline With copper(I) bromide in N,N-dimethyl-formamide T=110°C; 6 h;
参考文献
Shi, Liu; Liu, Xiangqian; Zhang, Hui; Jiang, Yongwen; Ma, Dawei
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 4200 - 4204
615-43-0
2-碘苯胺
+
10111-08-7
2-咪唑甲醛
→
反应条件
235-05-2
咪唑并[1,2-a]喹喔啉
反应条件
potassium phosphate; copper(l) iodide; (-)-sparteine in 1-methyl-pyrrolidin-2-one T=130°C; 24 h;
参考文献
Reeves, Jonathan T.; Fandrick, Daniel R.; Tan, Zhulin; Song, Jinhua J.; Lee, Heewon; Yee, Nathan K.; Senanayake, Chris H.
Journal of Organic Chemistry, 2010 , vol. 75, # 3 p. 992 - 994
615-43-0
2-碘苯胺
+
100-10-7
对二甲氨基苯甲醛
→
反应条件
2562-71-2
2-(p-N,N-二甲基氨基苯基)-1H-苯并咪唑
反应条件
sodium azide; N,N,N',N,-tetramethylethylenediamine; copper(l) chloride in dimethyl sulfoxide T=120°C; 12 h;
参考文献
Kim, Yong; Kumar, Manian Rajesh; Park, Namjin; Heo, Yumi; Lee, Sunwoo
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9577 - 9583
931-48-6
环己基乙炔
+
615-43-0
2-碘苯胺
→
反应条件
287477-26-3
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine in N,N-dimethyl-formamide T=50°C; Inert atmosphere;
参考文献
Peng, Changlan; Wang, Yong; Liu, Lanying; Wang, Honggen; Zhao, Jiaji; Zhu, Qiang
European Journal of Organic Chemistry, 2010 , # 5 p. 818 - 822
615-43-0
2-碘苯胺
+
109-46-6
N,N'-二丁基硫脲
→
反应条件
24622-31-9
N-丁基-(9ci)-2-氨基苯并噻唑
反应条件
Ni(PEt3)2Cl2; sodium cyanoborohydride in N,N-dimethyl-formamide T=60°C; 60 h;
参考文献
Takagi, Kentaro
Chemistry Letters, 1986 , p. 265 - 266
615-43-0
2-碘苯胺
+
592-82-5
→
反应条件
24622-31-9
N-丁基-(9ci)-2-氨基苯并噻唑
反应条件
copper(l) iodide; triethylamine in dimethyl sulfoxide T=80°C; 48 h;
参考文献
Sun, Ya-Lei; Zhang, Yuan; Cui, Xiao-Hui; Wang, Wei
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 7 p. 1174 - 1178
615-43-0
2-碘苯胺
+
614-69-7
→
反应条件
25717-12-8
反应条件
tetrabutylammomium bromide; copper(I) bromide in dimethyl sulfoxide T=40°C; 20 h;
参考文献
Guo, Yan-Jin; Tang, Ri-Yuan; Zhong, Ping; Li, Jin-Heng
Tetrahedron Letters, 2010 , vol. 51, # 4 p. 649 - 652
615-43-0
2-碘苯胺
→
反应条件
1912-33-0
反应条件
1.1: 100 percent / NaH / tetrahydrofuran / 24 h / 20 °C 2.1: 81 percent / Et3N; P(o-tol)3 / Pd(OAc)2 / acetonitrile / 2.5 h / Heating 3.1: 85 percent / triphosgene; Et3N / CH2Cl2 / 1 h / 0 - 20 °C 4.1: Bu3SnH; AIBN / acetonitrile / 100 °C 4.2: 56 percent / CuI; (2-bromo-4-methylphenyl)carbamic acid tert-butyl ester / Pd(PPh3)4 / dimethylformamide / 50 °C View Scheme
参考文献
Zhang, Han-Cheng; Maryanoff, Bruce E.
Journal of Organic Chemistry, 1997 , vol. 62, # 6 p. 1804 - 1809
201230-82-2
+
615-43-0
2-碘苯胺
+
98-80-6
→
反应条件
2835-77-0
反应条件
1: 2-iodo aniline; 3,4,5-trimethoxyphenylboronic acid With potassium carbonate in toluene Suzuki cross-coupling reaction; 0.166667 h; Autoclave; 2: carbon monoxide in toluene T=100°C; Suzuki cross-coupling reaction; P=5171.62 Torr; 10 h; Autoclave;
参考文献
Qureshi, Ziyauddin S.; Deshmukh, Krishna M.; Tambade, Pawan J.; Bhanage, Bhalchandra M.
Synthesis, 2011 , # 2 art. no. P15410SS, p. 243 - 250
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