palladium diacetate; tetrabutyl-ammonium chloride; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=100°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Larock; Yum; Refvik
Journal of Organic Chemistry, 1998 , vol. 63, # 22 p. 7652 - 7662
1.1: 72 percent / DMAP; pyridine / 18 h / Heating 2.1: NaH / dimethylformamide / 0.25 h / 20 °C 2.2: 47 percent / dimethylformamide / 4 h / 20 °C 3.1: 14.3 percent / 1-ethylpiperidine hypophosphite; AIBN / benzene / 1 h / Heating View Scheme
参考文献
Murphy, John A.; Scott, Karen A.; Sinclair, Rhoha S.; Martin, Concepcion Gonzalez; Kennedy, Alan R.; Lewis, Norman
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 15 p. 2395 - 2408
