1: pyridine / 3 h / 20 - 70 °C / Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0); tetra(n-butyl)ammonium hydrogensulfate; caesium carbonate / N,N-dimethyl-formamide; toluene / 18 h / 60 °C / Inert atmosphere
3: palladium diacetate; caesium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 12 h / 40 °C / Inert atmosphere
View Scheme
参考文献
Rixson, James E.; Chaloner, Thomas; Heath, Charles H.; Tietze, Lutz F.; Stewart, Scott G.
European Journal of Organic Chemistry, 2012 , # 3 p. 544 - 558
1: pyridine / 3 h / 20 - 70 °C / Inert atmosphere
2: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); potassium acetate / N,N-dimethyl-formamide / 120 °C / Inert atmosphere
View Scheme
参考文献
Rixson, James E.; Chaloner, Thomas; Heath, Charles H.; Tietze, Lutz F.; Stewart, Scott G.
European Journal of Organic Chemistry, 2012 , # 3 p. 544 - 558