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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘苯胺
合成路线
（共 712 条）
615-43-0
2-碘苯胺
+
93267-04-0
N-(叔-丁氧基羰基)-3-碘-L-丙氨酸甲酯
→
反应条件
166246-74-8
反应条件
1: N-[(1,1-dimethylethoxy)carbonyl]-3-iodo-L-alanine methyl ester With iodine; zinc in N,N-dimethyl-formamide T=20°C; Inert atmosphere; 2: 2-iodo aniline With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Ross, Andrew J.; Lang, Hannah L.; Jackson, Richard F. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 1 p. 245 - 248
617-89-0
2-呋喃甲胺
+
615-43-0
2-碘苯胺
→
反应条件
1569-98-8
2-(2-呋喃基)-苯并噻唑
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
98-01-1
糠醛
+
615-43-0
2-碘苯胺
→
反应条件
1569-98-8
2-(2-呋喃基)-苯并噻唑
反应条件
1,10-phenanthroline; CuCl2·2H2O; potassium carbonate; sulfur in water T=100°C; 24 h;
参考文献
Deng, Hang; Li, Zhengkai; Ke, Fang; Zhou, Xiangge
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4840 - 4843
615-43-0
2-碘苯胺
+
6006-81-1
beta-亚甲基苯乙醇
→
反应条件
1666-96-2
反应条件
sodium hydrogencarbonate; triphenylphosphine; palladium dichloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=140°C; 96 h;
参考文献
Larock, Richard C.; Kuo, Mann-Yan
Tetrahedron Letters, 1991 , vol. 32, # 5 p. 569 - 572
104-53-0
苯丙醛
+
615-43-0
2-碘苯胺
→
反应条件
16886-10-5
3-苄基吲哚
反应条件
1: 2-iodo aniline With AmPhos; palladium dichloride in 1,4-dioxane T=20°C; 0.166667 h; Inert atmosphere; 2: 3-phenyl-propionaldehyde With caesium acetate in 1,4-dioxane T=120°C; 0.666667 h; Inert atmosphereMicrowave irradiation;
参考文献
Karuvalam, Ranjith P.; Haridas, Karickal R.; Sajith, Ayyiliath M.; Muralidharan, Arayambath
Tetrahedron Letters, 2013 , vol. 54, # 37 p. 5126 - 5129
615-43-0
2-碘苯胺
→
反应条件
16886-10-5
3-苄基吲哚
反应条件
1: LDA / tetrahydrofuran / -78 °C 2: 78 percent / Cs2CO3 / Pd2(dba)3; 1,3-bis(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazolium / dimethylamine / 2 h / 140 °C View Scheme
参考文献
Fukuyama, Tohru; Chen, Xiaoqi; Peng, Ge
Journal of the American Chemical Society, 1994 , vol. 116, # 7 p. 3127 - 3128
615-43-0
2-碘苯胺
→
反应条件
1484-19-1
3-乙基吲哚
反应条件
1: LDA / tetrahydrofuran / -78 °C 2: 82 percent / Cs2CO3 / Pd2(dba)3; 1,3-bis(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazolium / dimethylamine / 1 h / 140 °C View Scheme
参考文献
Caddick, Stephen; Kofie, William
Tetrahedron Letters, 2002 , vol. 43, # 51 p. 9347 - 9350
201230-82-2
+
615-43-0
2-碘苯胺
+
536-74-3
→
反应条件
14802-18-7
反应条件
diethylamine; bis-triphenylphosphine-palladium(II) chloride T=120°C; 6 h; Pressure (range begins): 20 <unit not given>;
参考文献
Torii, Sigeru; Okumoto, Hiroshi; Xu, Long He; Sadakane, Masahiro; Shostakovsky, Michel V.; Ponomaryov, Andrew B.; Kalinin, Valery N.
Tetrahedron, 1993 , vol. 49, # 31 p. 6773 - 6784
615-43-0
2-碘苯胺
→
反应条件
1496-76-0
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 72 h / 20 °C / |Inert atmosphere 2: triethylamine / tetrahydrofuran / 16 h / 20 °C / |Inert atmosphere 3: caesium carbonate; FeCl3·6H2O; pyridine / toluene / 150 °C / |Sealed tube View Scheme
参考文献
Herrero, Maria Teresa; De Sarralde, Jokin Diaz; Sanmartin, Raul; Bravo, Laura; Dominguez, Esther
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 16 p. 3054 - 3064
615-43-0
2-碘苯胺
+
123-54-6
→
反应条件
22582-52-1
反应条件
copper(I) oxide; caesium carbonate in water; dimethyl sulfoxide T=100°C; 7 h; Inert atmosphere; regiospecific reaction;
参考文献
Ali, Md Ashif; Punniyamurthy, Tharmalingam
Synlett, 2011 , # 5 art. no. D26210ST, p. 623 - 626
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