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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘苯胺
合成路线
（共 712 条）
615-43-0
2-碘苯胺
+
122-78-1
苯乙醛
→
反应条件
5021-43-2
2-苯基喹噁啉
反应条件
copper(l) iodide; sodium azide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in dimethyl sulfoxide T=80°C; 20 h; Sealed tube; Catalytic behavior; TemperatureReagent/catalystTime; regioselective reaction;
参考文献
Yuan, Hua; Li, Kangning; Chen, Yongxin; Wang, Yu; Cui, Jiaojiao; Chen, Baohua
Synlett, 2013 , vol. 24, # 17 art. no. ST-2013-W0618-L, p. 2315 - 2319
5703-26-4
4-甲氧基苯乙醛
+
615-43-0
2-碘苯胺
→
反应条件
5021-46-5
反应条件
copper(l) iodide; sodium azide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in dimethyl sulfoxide T=80°C; 20 h; Sealed tube; regioselective reaction;
参考文献
Yuan, Hua; Li, Kangning; Chen, Yongxin; Wang, Yu; Cui, Jiaojiao; Chen, Baohua
Synlett, 2013 , vol. 24, # 17 art. no. ST-2013-W0618-L, p. 2315 - 2319
615-43-0
2-碘苯胺
→
反应条件
5026-42-6
5,10-二氢-5-甲基-11H-二苯并[b,e][1,4]二氮杂卓-11-酮
反应条件
1.1: t-BuOK / dimethylsulfoxide / 2 h / 20 °C 1.2: 1 h / 20 °C 2.1: SnCl2*2H2O / ethyl acetate / 18 h / 20 °C 3.1: 98 percent / diisopropylethylamine; palladium complexed dendrimer / toluene / 22 h / 80 °C / 5171.48 Torr View Scheme
参考文献
Lu, Shui-Ming; Alper, Howard
Journal of the American Chemical Society, 2005 , vol. 127, # 42 p. 14776 - 14784
615-43-0
2-碘苯胺
→
反应条件
53654-35-6
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 72 h / 20 °C / |Inert atmosphere 2: triethylamine / tetrahydrofuran / 16 h / 20 °C / |Inert atmosphere 3: caesium carbonate; FeCl3·6H2O; pyridine / toluene / 150 °C / |Sealed tube View Scheme
参考文献
Herrero, Maria Teresa; De Sarralde, Jokin Diaz; Sanmartin, Raul; Bravo, Laura; Dominguez, Esther
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 16 p. 3054 - 3064
615-43-0
2-碘苯胺
+
68-12-2
N,N-二甲基甲酰胺
→
反应条件
53666-10-7
反应条件
in N,N-dimethyl-formamide T=80°C; Inert atmosphere;
参考文献
Halim, Rosliana; Aurelio, Luigi; Scammells, Peter J.; Flynn, Bernard L.
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 4708 - 4718
615-43-0
2-碘苯胺
+
4637-24-5
N,N-二甲基甲酰胺二甲基缩醛
→
反应条件
53666-10-7
反应条件
in N,N-dimethyl-formamide T=80°C;
参考文献
Halim, Rosliana; Scammells, Peter J.; Flynn, Bernard L.
Organic Letters, 2008 , vol. 10, # 10 p. 1967 - 1970
766-47-2
2-乙炔基甲苯
+
615-43-0
2-碘苯胺
→
反应条件
537684-22-3
2-(2-甲基苯基)-1H-吲哚
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine in N,N-dimethyl acetamide T=20°C; Sonogashira Cross-Coupling; 1 h; 2: With sodium hydroxide in N,N-dimethyl acetamide T=140°C;
参考文献
Yu, Xufen; Park, Eun-Jung; Kondratyuk, Tamara P.; Pezzuto, John M.; Sun, Dianqing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 44 p. 8835 - 8847
615-43-0
2-碘苯胺
+
577-16-2
→
反应条件
537684-22-3
2-(2-甲基苯基)-1H-吲哚
反应条件
DiPPF; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate in 1,4-dioxane 20 h; Heating;
参考文献
Cho, Chan Sik; Kim, Jun Ho; Kim, Tae-Jeong; Shim, Sang Chul
Journal of Chemical Research, 2004 , # 9 p. 630 - 631
615-43-0
2-碘苯胺
→
反应条件
53786-47-3
反应条件
1: trifluoroacetic acid; sodium triacetoxyborohydride / isopropyl acetate / 0.17 h 2: tetrahydrofuran; isopropyl acetate / 0.5 h / cooling 3: water / tetrahydrofuran; isopropyl acetate / 0.67 h / -10 - 20 °C 4: 99 percent Chromat. / NaHCO3; H2O / Pd(OAc)2; X-Phos / propan-2-ol / 72 h / 83 °C View Scheme
参考文献
McLaughlin, Mark; Palucki, Michael; Davies, Ian W.
Organic Letters, 2006 , vol. 8, # 15 p. 3311 - 3314
4746-97-8
+
615-43-0
2-碘苯胺
→
反应条件
54621-12-4
反应条件
1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate in N,N-dimethyl-formamide T=105°C;
参考文献
Chen; Lieberman; Larsen; Verhoeven; Reider
Journal of Organic Chemistry, 1997 , vol. 62, # 9 p. 2676 - 2677
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