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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘苯胺
合成路线
（共 712 条）
615-43-0
2-碘苯胺
+
140-88-5
丙烯酸乙酯
→
反应条件
58106-56-2
反应条件
tetrabutylammomium bromide; palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=80°C; Heck Reaction; Inert atmosphere;
参考文献
Adepu, Raju; Rajitha; Ahuja, Dipali; Sharma, Atul Kumar; Ramudu; Kapavarapu, Ravikumar; Parsa, Kishore V. L.; Pal, Manojit
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 16 p. 2514 - 2518
925-60-0
丙烯酸正丙酯
+
615-43-0
2-碘苯胺
→
反应条件
58106-56-2
反应条件
triethylamine in N,N-dimethyl-formamide T=75°C; Heck Reaction; 20 h; Green chemistry;
参考文献
Basu, Basudeb; Paul, Susmita
Applied Organometallic Chemistry, 2013 , vol. 27, # 10 p. 588 - 594
615-43-0
2-碘苯胺
+
107-13-1
丙烯腈
→
反应条件
58106-57-3
反应条件
triethylamine; tris-(o-tolyl)phosphine; palladium diacetate in acetonitrile T=100°C; Heck reaction; 40 h;
参考文献
So, Won Youn; Song, Ju-Hyun; Jung, Dai-Il
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5658 - 5661
615-43-0
2-碘苯胺
→
反应条件
590372-08-0
反应条件
1: 41 percent / H2O / 6 h / 130 °C 2: 39 percent / H2SO4 (96 percent) / 0.83 h / 90 °C 3: 88 percent / POBr3 / 2 h / 150 °C View Scheme
参考文献
Marull, Marc; Lefebvre, Olivier; Schlosser, Manfred
European Journal of Organic Chemistry, 2004 , # 1 p. 54 - 63
615-43-0
2-碘苯胺
→
反应条件
59591-73-0
1H-吲唑-3-基苯基甲酮
反应条件
1.1: hydrogenchloride; sodium nitrite / acetonitrile; water / 0 - 5 °C 1.2: 1 h / 0 - 20 °C 2.1: tetrakis(triphenylphosphine) palladium(0); pyrrolidine / 60 °C / |Inert atmosphere 2.2: 10.5 h / 60 °C / |Inert atmosphere 3.1: copper (II) acetate monohydrate; oxygen / methanol / 90 °C / |Schlenk technique 4.1: ammonium cerium (IV) nitrate / methanol / 1 h View Scheme
参考文献
Fang, Yan; Wang, Chengming; Su, Shengqin; Yu, Haizhu; Huang, Yong
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 7 p. 1061 - 1071
615-43-0
2-碘苯胺
→
反应条件
6011-26-3
反应条件
1: tetrakis(triphenylphosphine) palladium(0); triethylamine; copper(I) bromide / toluene / 5 h / 20 °C / |Inert atmosphere; |Schlenk technique 2: triethylamine / tetrahydrofuran / 0.5 h / 20 °C 3: potassium fluoride / N,N-dimethyl-formamide; water / 0.5 h / 20 °C 4: tetrakis(triphenylphosphine) palladium(0); hydrogenchloride / tetrahydrofuran; water / 60 h / 45 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Xu, Caixia; Du, Weiyuan; Zeng, Yi; Dai, Bin; Guo, Hao
Organic Letters, 2014 , vol. 16, # 3 p. 948 - 951
1193-62-0
2-吡咯甲酸甲酯
+
615-43-0
2-碘苯胺
→
反应条件
74497-02-2
+
6025-68-9
吡咯并[1,2-a]喹喔啉-4(5H)-酮
反应条件
copper(l) iodide; potassium carbonate; L-proline in dimethyl sulfoxide T=80°C; 25 h;
参考文献
Yuan, Qiliang; Ma, Dawei
Journal of Organic Chemistry, 2008 , vol. 73, # 13 p. 5159 - 5162
766-96-1
(4-溴苯基)乙炔
+
615-43-0
2-碘苯胺
→
反应条件
6127-49-7
2-(4-溴苯基)-1H-吲哚
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine in N,N-dimethyl acetamide T=20°C; Sonogashira Cross-Coupling; 1 h; 2: With sodium hydroxide in N,N-dimethyl-aniline T=140°C;
参考文献
Yu, Xufen; Park, Eun-Jung; Kondratyuk, Tamara P.; Pezzuto, John M.; Sun, Dianqing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 44 p. 8835 - 8847
615-43-0
2-碘苯胺
→
反应条件
61403-29-0
反应条件
1: 80 percent / Et3N / CH2Cl2 / 0 °C 2: 79 percent / CuI; PPh3; Et3N / Pd2(dba)3 / 40 h / 50 °C 3: TBAF / tetrahydrofuran View Scheme
参考文献
Herrero, Maria Teresa; De Sarralde, Jokin Diaz; Sanmartin, Raul; Bravo, Laura; Dominguez, Esther
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 16 p. 3054 - 3064
615-43-0
2-碘苯胺
+
98-59-9
对甲苯磺酰氯
→
反应条件
61613-20-5
N-对甲苯磺酰基-2-碘苯胺
反应条件
pyridine in tetrahydrofuran T=20°C; 14 h; Inert atmosphere;
参考文献
Varela-Fernandez, Alejandro; Varela, Jesus A.; Saa, Carlos
Synthesis (Germany), 2012 , vol. 44, # 21 art. no. SS-2012-Z0414-PSP, p. 3285 - 3295
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