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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘苯胺
合成路线
（共 712 条）
615-43-0
2-碘苯胺
+
54060-30-9
3-氨基苯乙炔
→
反应条件
6318-72-5
3-(1H-吲哚-2-基)-苯胺
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine in N,N-dimethyl acetamide T=20°C; Sonogashira Cross-Coupling; 1 h; 2: With sodium hydroxide in N,N-dimethyl acetamide T=140°C;
参考文献
Yu, Xufen; Park, Eun-Jung; Kondratyuk, Tamara P.; Pezzuto, John M.; Sun, Dianqing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 44 p. 8835 - 8847
615-43-0
2-碘苯胺
+
100-39-0
溴化苄
→
反应条件
6325-92-4
反应条件
1: 2-iodo aniline With tert.-butyl lithium; isopropylmagnesium chloride in tetrahydrofuran; diethyl ether; pentane T=-78°C; 0.5 h; 2: With sulfur in tetrahydrofuran; diethyl ether; pentane T=-78 - 20°C; 0.5 h; 3: benzyl bromide in tetrahydrofuran; diethyl ether; pentane T=0 - 20°C;
参考文献
Ham, Jungyeob; Cho, Sung Jin; Ko, Jaeyoung; Chin, Jungwook; Kang, Heonjoong
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5781 - 5784
615-43-0
2-碘苯胺
→
反应条件
63359-54-6
2-乙烯基苯并[d]噁唑
反应条件
1: 87 percent / Et3N, 1-methyl-2-chloropyridinium iodide / CH2Cl2 / 8 h / Ambient temperature 2: 71 percent / NaH, CuI / dimethylformamide / 1.) r.t., 10 min, 2.) 100 deg C, 5 h 3: 20 percent / NaH / tetrahydrofuran / 1.) r.t., 10 min, 2.) 0 deg C, 1.5 h View Scheme
参考文献
Minami, Toru; Isonaka, Takeshi; Okada, Yoshiharu; Ichikawa, Junji
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7009 - 7015
615-43-0
2-碘苯胺
→
反应条件
64085-53-6
反应条件
sodium periodate; potassium iodide; sodium chloride in water; acetic acid T=25°C; 2 h;
参考文献
Emmanuvel, Lourdusamy; Shukla, Ravi Kant; Sudalai, Arumugam; Gurunath, Suryavanshi; Sivaram, Swaminathan
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4793 - 4796
615-43-0
2-碘苯胺
→
反应条件
64236-22-2
反应条件
1: MgSO4 / toluene / 100 °C 2: cesium pivalate / Pd(OAc)2; 1,1-bis(diphenylphosphino)methane / dimethylformamide / 24 h / 100 °C View Scheme
参考文献
Zhao, Jian; Yue, Dawei; Campo, Marino A.; Larock, Richard C.
Journal of the American Chemical Society, 2007 , vol. 129, # 16 p. 5288 - 5295
201230-82-2
+
615-43-0
2-碘苯胺
+
34918-74-6
→
反应条件
37856-17-0
反应条件
palladium diacetate; triethylamine; triphenylphosphine in tetrahydrofuran T=110°C; P=25858.1 Torr; 48 h; Autoclave;
参考文献
Zheng, Zhaoyan; Alper, Howard
Organic Letters, 2008 , vol. 10, # 5 p. 829 - 832
615-43-0
2-碘苯胺
→
反应条件
382156-92-5
反应条件
1: 91 percent / Pd(PPh3)2Cl2; CuI / triethylamine / 5 h / 60 °C 2: 88 percent / Et3N / diethyl ether / 1 h / 0 °C 3: 98 percent / KOH; Bu4NI / tetrahydrofuran / 5 h / sonication View Scheme
参考文献
Dominguez, Gema; Casarrubios, Luis; Rodriguez-Noriega, Javier; Perez-Castells, Javier
Helvetica Chimica Acta, 2002 , vol. 85, # 9 p. 2856 - 2861
1003-31-2
2-氰基噻吩
+
615-43-0
2-碘苯胺
→
反应条件
3878-18-0
(9ci)-2-(2-噻吩)-1H-苯并咪唑
反应条件
potassium tert-butylate in N,N-dimethyl acetamide T=100°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Xiang, Shi-Kai; Tan, Wen; Zhang, Dong-Xue; Tian, Xian-Li; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 42 p. 7271 - 7275
98-03-3
2-噻吩甲醛
+
615-43-0
2-碘苯胺
→
反应条件
3878-18-0
(9ci)-2-(2-噻吩)-1H-苯并咪唑
反应条件
sodium azide; N,N,N',N,-tetramethylethylenediamine; copper(l) chloride in dimethyl sulfoxide T=120°C; 12 h;
参考文献
Kim, Yong; Kumar, Manian Rajesh; Park, Namjin; Heo, Yumi; Lee, Sunwoo
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9577 - 9583
201230-82-2
+
615-43-0
2-碘苯胺
+
15999-95-8
→
反应条件
37856-14-7
反应条件
palladium diacetate; triethylamine; triphenylphosphine in tetrahydrofuran T=110°C; P=25858.1 Torr; 48 h; Autoclave;
参考文献
Zheng, Zhaoyan; Alper, Howard
Organic Letters, 2008 , vol. 10, # 5 p. 829 - 832
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