反应条件
1.1: bis(triphenylphosphine)palladium(II)chloride; copper(I) iodide; triethylamine / 25 - 50 °C
2.1: iodomethane / 120 °C
3.1: 88 percent / copper(I) iodide; triethylamine; PdCl2(PPh3)2
4.1: iodomethane / 120 °C
5.1: copper(I) iodide; triethylamine; PdCl2(PPh3)2
6.1: iodomethane / 120 °C
7.1: potassium carbonate / methanol; diethyl ether
8.1: tetrabutylammonium fluoride / tetrahydrofuran / 20 °C
8.2: copper(I) iodide; bis(dibenzylideneacetone)palladium(0); triphenylphosphine / triethylamine
View Scheme
参考文献
Kehoe, Joshua M.; Kiley, James H.; English, Jamieson J.; Johnson, Charles A.; Petersen, Ryan C.; Haley, Michael M.
Organic Letters, 2000 , vol. 2, # 7 p. 969 - 972