2,2-二甲基-1-苯丙胺合成路线 （共 19 条）
反应条件
1: 100 percent / diethyl ether / 3 h / Ambient temperature 2: 1.) PPh3 / 1.) Et2), RT, 4 h, 2.) Et2O, RT, overnight 3: 1.) aq. KOH, 2.) 10percent aq. HCl / 1.) EtOH, RT, 1 h, 2.) EtOH, reflux, 2 h View Scheme
参考文献
Synthetic Communications, , vol. 24, # 20 p. 2955 - 2972
反应条件
hydrogenchloride 1 h; Heating;
参考文献
Chemistry - A European Journal, , vol. 11, # 19 p. 5619 - 5624
反应条件
zinc(II) tetrahydroborate 1) Et2O, reflux, 20 h, 2) 0 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 5 p. 401 - 402
反应条件
hydrogenchloride; potassium hydroxide 1.) EtOH, RT, 1 h, 2.) EtOH, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 24, # 20 p. 2955 - 2972
反应条件
1: 1.) PPh3 / 1.) Et2), RT, 4 h, 2.) Et2O, RT, overnight 2: 1.) aq. KOH, 2.) 10percent aq. HCl / 1.) EtOH, RT, 1 h, 2.) EtOH, reflux, 2 h View Scheme
参考文献
Synthetic Communications, , vol. 24, # 20 p. 2955 - 2972
反应条件
lithium aluminium tetrahydride; copper(l) chloride 1.) THF, reflux, 6 h, 2.) reflux, 3 h; r.t., 15 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 7 p. 691 - 703
反应条件
(i) Et2O, (ii) H2O; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 42, # 2 p. 398 - 399
反应条件
aschliessendes Hydrolysieren;
参考文献
Anales de la Real Sociedad Espanola de Fisica y Quimica, Serie B: Quimica, , vol. 50, p. 875,884
参考文献
Cervinka,O.; Fusek,J.
Collection of Czechoslovak Chemical Communications, 1973 , vol. 38, p. 441 - 446
