5-甲氧基-2,4-二氮杂双环[4.3.0]壬-2,4,10-三烯-3-胺合成路线 (共 6 条)
反应条件
in methanol; xylene
3 h; Heating / reflux;
参考文献
Wyeth
Patent: US2006/276446 A1, 2006 ;
Location in patent: Page/Page column 28 ;
US 20060276446 A1
反应条件
in xylene
3 h; Heating / reflux;
参考文献
WYETH
Patent: WO2003/93280 A1, 2003 ;
Location in patent: Page/Page column 148 ;
反应条件
methanol; sodium methylate; xylene
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111
Full Text Show Details
Braker et al.
Journal of the American Chemical Society, 1947 , vol. 69, p. 3072,3075
反应条件
1: POCl3
2: methanol; O,O'-dimethyl-diethylene glycol
View Scheme
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111
反应条件
1: ethanol
2: POCl3
3: methanol; O,O'-dimethyl-diethylene glycol
View Scheme
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111
反应条件
methanol; diethylene glycol dimethyl ether
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111