2-甲基-5-氨基-2H-四氮唑合成路线 (共 18 条)
反应条件
hydrogen; palladium dihydroxide in ethanol T=50°C; P=2585.81 Torr; 16 h;
参考文献
Pfizer Inc
Patent: US2007/213371 A1, 2007 ;
Location in patent: Page/Page column 100 ;
反应条件
hydrogen; palladium dihydroxide in ethanol T=50°C; P=2585.81 Torr; 16 h;
参考文献
US2007/213314 A1, ;
Page/Page column 118 ;
反应条件
1: 5-amino-1H-tetrazole With 3,3-bis(4'-hydroxyphenyl)-phthalide; sodium hydroxide in water 2: dimethyl sulfate With sodium hydroxide in water 1 h; Reflux;
参考文献
Journal of Molecular Structure, , vol. 1023, p. 128 - 142
反应条件
1: 5-amino-2H-tetrazole With sodium hydroxide in water 2: dimethyl sulfate in N,N-dimethyl-formamide 4 h; Reflux;
参考文献
Fendt, Tobias; Fischer, Niko; Klapoetke, Thomas M.; Stierstorfer, Joerg
Inorganic Chemistry, 2011 , vol. 50, # 4 p. 1447 - 1458
反应条件
sodium hydroxide in water; acetone 3 h; Heating; Yield given;
参考文献
Australian Journal of Chemistry, , vol. 37, # 12 p. 2453 - 2468
反应条件
1: With hydrazine hydrate in ethanol 2 h; Reflux; 2: With acetic acid in ethanol 1 h; Reflux;
参考文献
Klapoetke, Thomas M.; Sabate, Carles Miro; Penger, Alexander; Rusan, Magdalena; Welch, Jan M.
European Journal of Inorganic Chemistry, 2009 , # 7 p. 880 - 896
反应条件
methanol; platinum Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 923,924
参考文献
Journal of the American Chemical Society, , vol. 78, p. 411,414
参考文献
Journal of the American Chemical Society, , vol. 76, p. 923,924
参考文献
Journal of the American Chemical Society, , vol. 78, p. 411,414