二甲基二硫代氨基甲酸氰基甲基酯合成路线 （共 29 条）
反应条件
sodium hydroxide 1.) DMSO, 18 deg C, 5 min; 2.) 18 deg C, 50 min; Yield given. Multistep reaction;
参考文献
Makosza, M.; Ludwiczak, S.
Synthesis, 1986 , # 1 p. 50 - 52
反应条件
potassium tert-butylate in tetrahydrofuran T=-20 - -10°C; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Makosza, Mieczyslaw; Wenaell, Maria; Golinski, Miroslaw; Kinowski, Andrzej
Bulletin of the Polish Academy of Sciences, Chemistry, 1985 , vol. 33, # 9-10 p. 427 - 432
参考文献
Journal of Organic Chemistry, , vol. 45, # 8 p. 1534 - 1535
反应条件
1: concentrated sulfuric acid / anschliessendes Behandeln mit wss.Natriumcarbonat-Loesung 2: sulfuric acid View Scheme
参考文献
Nachmias
Annales de Chimie (Cachan, France), 1952 , vol. <12> 7, p. 584,599
参考文献
Journal of Organic Chemistry, , vol. 45, # 8 p. 1534 - 1535
反应条件
potassium tert-butylate in tetrahydrofuran T=-20 - -10°C; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Makosza, Mieczyslaw; Wenaell, Maria; Golinski, Miroslaw; Kinowski, Andrzej
Bulletin of the Polish Academy of Sciences, Chemistry, 1985 , vol. 33, # 9-10 p. 427 - 432
反应条件
in ethanol
0.5 h; Ambient temperature;
参考文献
Harris, Roger L.N.; McFadden, Helen G.
Synthesis, 1985 , # 2 p. 209 - 210
参考文献
Yanagawa, Makato; Moriya, Osamu; Watanabe, Yoshihiko; Ueno, Yoshio; Endo, Takeshi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 2203 - 2204
参考文献
Doelling, Wolfgang; Sperk, Katrin; Augustin, Manfred
Journal fuer Praktische Chemie (Leipzig), 1990 , vol. 332, # 5 p. 671 - 678
反应条件
1: concentrated sulfuric acid / anschliessendes Behandeln mit wss.Natriumcarbonat-Loesung
2: unter Entfernen des entstehenden Wassers
View Scheme
参考文献
Nachmias
Annales de Chimie (Cachan, France), 1952 , vol. <12> 7, p. 584,599
