(1R,2S)-顺-2-羟基环戊羧酸乙酯合成路线 （共 20 条）
反应条件
(11bS, 11'bS)-4,4'-(oxydi-2,1-phenylene)bis-dinaphtho[2,1-d:,1',2'-f][1,3,2]dioxaphosphepin; hydrogen; [Ru(II)(η6-benzene)(μ-Cl)Cl]2 in ethanol; dichloromethane T=60°C; P=45003.6 Torr; 20 h; Title compound not separated from byproducts;
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 10-11 p. 1157 - 1160
反应条件
in ethanol T=25°C; prepared by Geotrichum candidum;
参考文献
Cossy, Janine; Ibhi, Said; Kahn, Philippe H.; Tacchini, Laura
Tetrahedron Letters, 1995 , vol. 36, # 43 p. 7877 - 7880
反应条件
Candida antarctica lipase B; water in tert-butyl methyl ether T=30°C; 1 h; Resolution of racemateEnzymatic reaction; Reagent/catalystSolventTemperature; enantioselective reaction;
参考文献
Forro, Eniko; Galla, Zsolt; Fueloep, Ferenc
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 98, p. 92 - 97
反应条件
hydrogen; [(R)-BINAP]RuBr2 in methanol T=80°C; P=76000 Torr; 48 h; variation of catalyst; Product distribution;
参考文献
Tetrahedron Letters, , vol. 35, # 26 p. 4559 - 4562
反应条件
glucose-6-phosphate dehydrogenase; G6P; nicotinamide adenine dinucleotide phosphate; Saccharomyces cerevisiae YDR368w dehydrogenase in phosphate buffer T=30°C; pH=7.0; 24 h;
参考文献
Tetrahedron Asymmetry, , vol. 18, # 18 p. 2133 - 2138
反应条件
Candida antarctica lipase B in various solvent(s) T=30°C; 2.66667 h;
参考文献
Tetrahedron Asymmetry, , vol. 14, # 14 p. 2053 - 2058
反应条件
immibilized baker's yeast; 1-n-butyl-3-methylimidazolium hexafluorophosphate; calcium alginate in methanol; water T=33°C; 72 h;
参考文献
Tetrahedron Letters, , vol. 42, # 42 p. 7517 - 7519
反应条件
Candida antarctica lipase B; water in tert-butyl methyl ether T=30°C; 0.5 h; Resolution of racemateEnzymatic reaction; enantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 98, p. 92 - 97
反应条件
1: vinyl acetate; ethyl cis-(±)-2-hydroxycyclopentane-1-carboxylate With Candida antarctica lipase B; water in tert-butyl methyl ether T=30°C; 0.5 h; Resolution of racemateEnzymatic reaction; 2: diazomethane enantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 98, p. 92 - 97
