alpha-氧代-苯乙酸环己基酯合成路线 （共 17 条）
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; 24 h;
参考文献
Szori, Kornel; Balazsik, Katalin; Felfoeldi, Karoly; Bartok, Mihaly
Journal of Catalysis, 2006 , vol. 241, # 1 p. 149 - 154
反应条件
1: Fe2(SO4)3*xH2O / Heating
2: 69 percent / ammonium chloroformate/alumina / cyclohexane / 1.5 h / 60 °C
View Scheme
参考文献
Zhang, Gui-Sheng; Gong, Hui
Synthetic Communications, 1999 , vol. 29, # 18 p. 3149 - 3153
反应条件
1: Fe2(SO4)3*xH2O / Heating
2: 69 percent / ammonium chloroformate/alumina / cyclohexane / 1.5 h / 60 °C
View Scheme
参考文献
Zhang, Gui-Sheng; Gong, Hui
Synthetic Communications, 1999 , vol. 29, # 18 p. 3149 - 3153
反应条件
1: oxalyl chloride; DMF / CH2Cl2 / 4 h / 20 °C
2: 4-dimethylaminopyridine; triethylamine / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Szori, Kornel; Balazsik, Katalin; Felfoeldi, Karoly; Bartok, Mihaly
Journal of Catalysis, 2006 , vol. 241, # 1 p. 149 - 154
反应条件
1.1: bromine / 1,4-dioxane / 25 - 30 °C / Inert atmosphere
2.1: dimethyl sulfoxide / 70 - 75 °C / Inert atmosphere
2.2: 25 - 30 °C / Inert atmosphere
View Scheme
参考文献
Raghunadh, Akula; Meruva, Suresh Babu; Kumar, Nuka Anil; Kumar, Gudla Santosh; Rao, L. Vaikunta; Syamkumar
Synthesis, 2012 , vol. 2012, # 2 p. 283 - 289
反应条件
1: toluene / 18 h / Reflux
2: triethylamine / dichloromethane / 80 °C / 12929 Torr
3: dirhodium(II) tetraoctanoate; water / dichloromethane
View Scheme
参考文献
Bartrum, Hannah E.; Blakemore, David C.; Moody, Christopher J.; Hayes, Christopher J.
Chemistry - A European Journal, 2011 , vol. 17, # 35 p. 9586 - 9589
反应条件
in benzene
Irradiation;
参考文献
Aoyama; Sakamoto; Kuwabara; Yoshida; Omote
Journal of the American Chemical Society, 1983 , vol. 105, # 7 p. 1958 - 1964
