13,14-二羟基二十二烷酸合成路线 （共 13 条）
反应条件
1: 3.17 g / NaIO4 / H2O; CHCl3 / 6 h / 20 °C
2: 95 percent / sodium borohydride / ethanol / 2 h / 20 °C
View Scheme
参考文献
Bieniarz, Christopher; Ramakrishna, Kornepati V.; Kelly, Terence P.
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 3 p. 243 - 250
反应条件
1: (esterification)
2: aq. NaIO4
3: Zn
4: P2O5
5: H2 / Raney-Ni
6: Na / xylene
View Scheme
参考文献
Dhekne,V.V. et al.
Indian Journal of Chemistry, 1966 , vol. 4, p. 524 - 526
反应条件
1: 89 percent / aq. Na2CO3, H3PO4, NaIO4
2: 1.) NaH, DMSO
3: PTS
4: 90 percent / LiAlH4 (LAH) / diethyl ether
5: 100 percent / pyridine / 24 h / Ambient temperature
View Scheme
参考文献
Subbaraman, A S; Mithran, S; Mamdapur, V R
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 865 - 866
