反应条件
carbon dioxide; methyl iodide in N,N-dimethyl-formamide; toluene byproducts: CsI; (Ar); standard Schlenk technique; toluene (1 equiv.), MeI (2 equiv.) and CsF (1.4 equiv.) added to soln. of tin compd. (1 equiv.) in DMF under CO2 at 19°C; GC and NMR monitoring; not isolated;
参考文献
Organometallics, , vol. 19, # 22 p. 4563 - 4567