反应条件
1: 5.8 g / 1.) n-BuLi, TMEDA / 1.) THF, 2.) -15 deg C, 1 h; 20 deg C, 2 h 2: 77 percent / H2SO4 conc. / 4 h / Heating 3: 1.64 g / 1.) n-BuLi / 1.) Et2O, reflux, 1 h, 2.) THF 4: 0.21 g / LiOH / H2O / 8 h / 25 °C / electrochemical reduction 5: diethyl ether / 0.5 h / 0 °C 6: m-CPBA / CH2Cl2 / 12 h / 0 °C View Scheme
参考文献
Lozanova, A. V.; Gul'tyai, V. P.; Karaseva, A. N.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, p. 1241 - 1245
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 6 p. 1370 - 1373
