1: 1-methyl-1H-imidazole With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.75 h; Inert atmosphere;
2: ethyl acetate in tetrahydrofuran; hexane
T=-78 - 20°C; 3 h; Inert atmosphere;
参考文献
Willemsen, Jorgen S.; Megens, Rik P.; Roelfes, Gerard; Van Hest, Jan C. M.; Rutjes, Floris P. J. T.
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2892 - 2898