4,6-二硝基-1,3-二甲苯合成路线 (共 35 条)
反应条件
nitrogen(IV) oxide; ozone in dichloromethane
T=-10°C; 3 h;
参考文献
Suzuki, Hitomi; Murashima, Takashi; Kozai, Iku; Mori, Tadashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 14 p. 1591 - 1598
参考文献
Davies; Hickox
Journal of the Chemical Society, 1922 , vol. 121, p. 2649
反应条件
1: diethyl ether
2: acetic acid; sulfuric acid
3: beim Schmelzen
View Scheme
参考文献
Borsche; Fiedler
Chemische Berichte, 1913 , vol. 46, p. 2125
反应条件
1: acetic acid; sulfuric acid
2: beim Schmelzen
View Scheme
参考文献
Borsche; Fiedler
Chemische Berichte, 1913 , vol. 46, p. 2125
反应条件
1: benzene
2: concentrated hydrochloric acid; alcohol
3: 170 °C
View Scheme
参考文献
Davies; Hickox
Journal of the Chemical Society, 1922 , vol. 121, p. 2649
反应条件
1: thionyl chloride / 190 - 200 °C / im Rohr
2: HNO3+H2SO4
3: benzene
4: concentrated hydrochloric acid; alcohol
5: 170 °C
View Scheme
参考文献
Davies; Hickox
Journal of the Chemical Society, 1922 , vol. 121, p. 2649
反应条件
1: concentrated hydrochloric acid; alcohol
2: 170 °C
View Scheme
参考文献
Davies; Hickox
Journal of the Chemical Society, 1922 , vol. 121, p. 2649
反应条件
1: HNO3+H2SO4
2: benzene
3: concentrated hydrochloric acid; alcohol
4: 170 °C
View Scheme
参考文献
Davies; Hickox
Journal of the Chemical Society, 1922 , vol. 121, p. 2649
参考文献
Boon
Journal of the Chemical Society, 1949 , p. Spl. 231
Full Text Show Details
Grieve; Hey
Journal of the Chemical Society, 1932 , p. 2245,2247
Full Text Show Details
Chang; Adams
Journal of the American Chemical Society, 1934 , vol. 56, p. 2089,2090
反应条件
in benzene
T=340°C; in sealed tube; other solvent (neat); other temp.; Product distributionKineticsRate constant;
参考文献
Oxley, Jimmie C.; Smith, James L.; Ye, Hong; McKenney, Robert L.; Bolduc, Paul R.
Journal of Physical Chemistry, 1995 , vol. 99, # 23 p. 9593 - 9602