2-氨基-5-硝基苯甲酸合成路线 (共 87 条)
反应条件
1: With copper(l) iodide; sodium azide; ethanol; caesium carbonate T=20 - 95°C; Inert atmosphereSealed tube; 2: With hydrogenchloride in water pH=2 - 3;
参考文献
Journal of Organic Chemistry, , vol. 75, # 10 p. 3311 - 3316
反应条件
4-amino-1,2,4-(4H)triazole; potassium tert-butylate in dimethyl sulfoxide 4 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 51, # 25 p. 5039 - 5040
反应条件
1: With potassium hydroxide; dihydrogen peroxide 0.5 h; cooling; 2: With sulfuric acid T=20°C; pH=1 - 2;
参考文献
Journal of Heterocyclic Chemistry, , vol. 41, # 4 p. 633 - 636
反应条件
methoxylamine hydrochloride; potassium tert-butylate; copper diacetate in ethylene glycol dimethyl ether T=20°C; Substitution; Amination;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 11 p. 1437 - 1444
反应条件
potassium chloride; water in acetonitrile T=70°C; also with D2O; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 115, # 24 p. 11358 - 11363
反应条件
ammonia; potassium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=150°C; 1 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 6, # 13 p. 1483 - 1486
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Journal of the American Chemical Society, , vol. 65, p. 1802
反应条件
sodium hydroxide; acetic acid 6 h; Heating;
参考文献
Magnetic Resonance in Chemistry, , vol. 27, # 11 p. 1007 - 1011
反应条件
potassium tert-butylate; 1,1,1-trimethylhydrazinium iodide in dimethyl sulfoxide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 9 p. 2934 - 2935
反应条件
ammonia T=130 - 160°C; Kochen des Produkts mit Barytwasser;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 195, p. 37
Chemische Berichte, , vol. 8, p. 1218