4-甲基伞型酮-beta-D-葡糖苷酸合成路线 （共 13 条）
反应条件
barium dimethoxide in methanol T=0 - 5°C; 24 h;
参考文献
Lopez-Lopez, Miguel A.; Balbuzano-Deus, Alexander; Rodriguez-Dominguez, Juan C.; Hernandez, Miriam Mesa; Villalobo, Anais Fernandez; Reyes, Yulianela Ibarra; Kirsch, Gilbert
Synlett, 2007 , # 4 p. 649 - 651
反应条件
oxygen; sodium hydrogencarbonate; platinum T=90°C;
参考文献
Nature (London, United Kingdom), , vol. 178, p. 589
反应条件
lithium hydroxide in tetrahydrofuran; water T=20°C; 1 h;
参考文献
Park, Sungjin; Shin, Injae
Organic Letters, 2007 , vol. 9, # 4 p. 619 - 622
反应条件
rat liver microsome solution; magnesium chloride in various solvent(s) T=37°C; pH=7.4; 0.166667 h;
参考文献
Analytical Chemistry, , vol. 78, # 20 p. 7071 - 7077
反应条件
1: 68 percent / aqueous sodium hypochlorite; TBAB; NaBr / 2,2,6,6-tetramethyl-1-piperidinyloxy; tetrabutylammonium bromide / aq. NaHCO3; CH2Cl2 / 3 h / 0 °C 2: 85 percent / barium methoxide / methanol / 24 h / 0 - 5 °C View Scheme
参考文献
Synlett, , # 4 p. 649 - 651
反应条件
1: 92 percent / iodine; methanol / benzene / 24 h / 65 °C 2: 68 percent / aqueous sodium hypochlorite; TBAB; NaBr / 2,2,6,6-tetramethyl-1-piperidinyloxy; tetrabutylammonium bromide / aq. NaHCO3; CH2Cl2 / 3 h / 0 °C 3: 85 percent / barium methoxide / methanol / 24 h / 0 - 5 °C View Scheme
参考文献
Synlett, , # 4 p. 649 - 651
反应条件
1: 45 percent / benzyltriethylammonium chloride; aq. NaOH / CHCl3 / 5 h / Heating 2: NaOMe; MeOH / 1 h / 20 °C 3: 0.068 mmol / LiOH / tetrahydrofuran; H2O / 1 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 9, # 4 p. 619 - 622
反应条件
1: NaOMe; MeOH / 1 h / 20 °C 2: 0.068 mmol / LiOH / tetrahydrofuran; H2O / 1 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 9, # 4 p. 619 - 622
反应条件
1: 45 percent / benzyltriethylammonium chloride; aq. NaOH / CHCl3 / 5 h / Heating 2: NaOMe; MeOH / 1 h / 20 °C 3: 0.068 mmol / LiOH / tetrahydrofuran; H2O / 1 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 9, # 4 p. 619 - 622
反应条件
magnesium chloride in phosphate buffer T=37°C; pH=7.4; 1.25 h; Enzyme kinetics; Further Variations:Solvents;
参考文献
Molecular Pharmacology, , vol. 72, # 4 p. 1054 - 1062
