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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
61603-51-8
合成路线
（共 13 条）
61603-52-9
→
反应条件
61603-51-8
反应条件
pyridinium hydrobromide perbromide in tetrahydrofuran 1 h;
参考文献
Davalian, Dariush; Garratt, Peter J.; Koller, Wolfgang; Mansuri, Muzammil M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4183 - 4193
515-84-4
三氯乙酸乙酯
+
5910-32-7
→
反应条件
61603-51-8
反应条件
sodium methylate in Petroleum ether 1.) 0 deg C, 2 h; 2.) RT, 15 h;
参考文献
Mueller, Paul; Rey, Michel
Helvetica Chimica Acta, 1982 , vol. 65, # 4 p. 1157 - 1166
4841-85-4
顺-4-环己烯-1,2-二羧酸二乙酯
→
反应条件
61603-51-8
反应条件
1: 84 percent / 50percent NaOH, Et3PhCH2NCl / 6 h / 40 - 50 °C 2: 66 percent / LiAlH4 / diethyl ether / 8 h / Ambient temperature 3: 18 percent / SOCl2 / pyridine / 1.) 0 deg C, 30 min; 2.) reflux, 20 min 4: 45 percent / KO-t-Bu / tetrahydrofuran / 1.5 h 5: 60 percent / CH2Cl2 / 2.5 h / Heating 6: 60 percent / pyridinium hydrobromide perbromide / tetrahydrofuran / 1 h View Scheme
参考文献
Davalian, Dariush; Garratt, Peter J.; Koller, Wolfgang; Mansuri, Muzammil M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4183 - 4193
57867-53-5
→
反应条件
61603-51-8
反应条件
1: 18 percent / SOCl2 / pyridine / 1.) 0 deg C, 30 min; 2.) reflux, 20 min 2: 45 percent / KO-t-Bu / tetrahydrofuran / 1.5 h 3: 60 percent / CH2Cl2 / 2.5 h / Heating 4: 60 percent / pyridinium hydrobromide perbromide / tetrahydrofuran / 1 h View Scheme
参考文献
Davalian, Dariush; Garratt, Peter J.; Koller, Wolfgang; Mansuri, Muzammil M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4183 - 4193
57867-52-4
→
反应条件
61603-51-8
反应条件
1: 66 percent / LiAlH4 / diethyl ether / 8 h / Ambient temperature 2: 18 percent / SOCl2 / pyridine / 1.) 0 deg C, 30 min; 2.) reflux, 20 min 3: 45 percent / KO-t-Bu / tetrahydrofuran / 1.5 h 4: 60 percent / CH2Cl2 / 2.5 h / Heating 5: 60 percent / pyridinium hydrobromide perbromide / tetrahydrofuran / 1 h View Scheme
参考文献
Davalian, Dariush; Garratt, Peter J.; Koller, Wolfgang; Mansuri, Muzammil M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4183 - 4193
57867-56-8
→
反应条件
61603-51-8
反应条件
1: 60 percent / CH2Cl2 / 2.5 h / Heating 2: 60 percent / pyridinium hydrobromide perbromide / tetrahydrofuran / 1 h View Scheme
参考文献
Davalian, Dariush; Garratt, Peter J.; Koller, Wolfgang; Mansuri, Muzammil M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4183 - 4193
74725-30-7
→
反应条件
61603-51-8
反应条件
1: 95 percent / 0.08 h / 200 °C / 14 Torr 2: 60 percent / CH2Cl2 / 2.5 h / Heating 3: 60 percent / pyridinium hydrobromide perbromide / tetrahydrofuran / 1 h View Scheme
参考文献
Davalian, Dariush; Garratt, Peter J.; Koller, Wolfgang; Mansuri, Muzammil M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4183 - 4193
57867-55-7
→
反应条件
61603-51-8
反应条件
1: 45 percent / KO-t-Bu / tetrahydrofuran / 1.5 h 2: 60 percent / CH2Cl2 / 2.5 h / Heating 3: 60 percent / pyridinium hydrobromide perbromide / tetrahydrofuran / 1 h View Scheme
参考文献
Davalian, Dariush; Garratt, Peter J.; Koller, Wolfgang; Mansuri, Muzammil M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4183 - 4193
57867-54-6
→
反应条件
61603-51-8
反应条件
1: 65 percent / KO-t-Bu / tetrahydrofuran / 1.5 h 2: 60 percent / CH2Cl2 / 2.5 h / Heating 3: 60 percent / pyridinium hydrobromide perbromide / tetrahydrofuran / 1 h View Scheme
参考文献
Davalian, Dariush; Garratt, Peter J.; Koller, Wolfgang; Mansuri, Muzammil M.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4183 - 4193
573-57-9
1,4-二氢-1,4-环氧萘
→
反应条件
61603-51-8
反应条件
1: 95 percent / 15 h / 140 - 145 °C / autoclave 2: 90 percent / conc. HCl / methanol / 15 h / Heating 3: 45 percent / CH3ONa / petroleum ether / 1.) 0 deg C, 2 h; 2.) RT, 15 h View Scheme
参考文献
Mueller, Paul; Rey, Michel
Helvetica Chimica Acta, 1982 , vol. 65, # 4 p. 1157 - 1166
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