3,5-二-o-乙酰基-5-溴-2-脱氧-d-尿苷合成路线 (共 3 条)
反应条件
N-bromosuccinmide; sodium azide in ethylene glycol dimethyl ether; water T=25°C; 24 h;
参考文献
Kumar; Wiebe; Knaus
Canadian Journal of Chemistry, 1994 , vol. 72, # 9 p. 2005 - 2010
反应条件
1-methyl-1H-imidazole in acetonitrile T=60°C; 1 h;
参考文献
Ortega, Jose-Antonio; Blas, Jose Ramon; Orozco, Modesto; Grandas, Anna; Pedroso, Enrique; Robles, Jordi
Organic Letters, 2007 , vol. 9, # 22 p. 4503 - 4506
反应条件
sodium methylate in methanol 1 h; Ambient temperature;
参考文献
Asakura, Jun-ichi; Robins, Morris J.
Journal of Organic Chemistry, 1990 , vol. 55, # 16 p. 4928 - 4933