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乙二醇
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63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3,3-二甲氧基联苯
合成路线
（共 68 条）
95149-16-9
+
1191415-07-2
→
反应条件
6161-50-8
3,3-二甲氧基联苯
+
1448818-00-5
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide T=90°C; 4 h; Inert atmosphereSchlenk technique; chemoselective reaction;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
European Journal of Organic Chemistry, 2013 , # 4 p. 781 - 788
95149-16-9
+
95186-48-4
→
反应条件
6161-50-8
3,3-二甲氧基联苯
+
1448818-04-9
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide T=90°C; 4 h; Inert atmosphereSchlenk technique; chemoselective reaction;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
European Journal of Organic Chemistry, 2013 , # 4 p. 781 - 788
95149-16-9
+
91703-34-3
→
反应条件
26870-34-8
+
6161-50-8
3,3-二甲氧基联苯
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide T=90°C; 4 h; Inert atmosphereSchlenk technique; chemoselective reaction;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
European Journal of Organic Chemistry, 2013 , # 4 p. 781 - 788
2398-37-0
间溴苯甲醚
+
98-56-6
对氯三氟甲苯
→
反应条件
581-80-6
+
6161-50-8
3,3-二甲氧基联苯
+
122801-56-3
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy in tetrahydrofuran T=63°C; 2 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
95149-16-9
+
103-80-0
→
反应条件
6161-50-8
3,3-二甲氧基联苯
+
62381-24-2
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in tetrahydrofuran T=80°C; 3 h; Schlenk tubeInert atmosphere;
参考文献
Rao, Maddali L.N.; Giri, Somnath; Jadhav, Deepak N.
Tetrahedron Letters, 2009 , vol. 50, # 45 p. 6133 - 6138
2398-37-0
间溴苯甲醚
+
78-93-3
→
反应条件
6161-50-8
3,3-二甲氧基联苯
+
1477782-02-7
反应条件
1: 3-methoxybromobenzene With iodine; magnesium in 2-methyl tetrahydrofuran T=40 - 45°C; 1.16667 h; Inert atmosphere; 2: butanone in 2-methyl tetrahydrofuran T=0°C; 4 h; Inert atmosphere; SolventTemperatureReagent/catalyst; chemoselective reaction;
参考文献
Kadam, Asha; Nguyen, Mylinh; Kopach, Michael; Richardson, Paul; Gallou, Fabrice; Wan, Zhao-Kui; Zhang, Wei
Green Chemistry, 2013 , vol. 15, # 7 p. 1880 - 1888
766-85-8
+
10365-98-7
→
反应条件
6161-50-8
3,3-二甲氧基联苯
反应条件
palladium 10 on activated carbon; potassium carbonate in water T=80°C; Suzuki-Miyaura Coupling; 2.5 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Riemer, Martin
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4104 - 4118
766-85-8
+
5798-75-4
→
反应条件
93-89-0
+
47230-38-6
+
6161-50-8
3,3-二甲氧基联苯
+
155061-61-3
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
766-85-8
+
927-77-5
→
反应条件
24743-14-4
+
20112-91-8
+
6161-50-8
3,3-二甲氧基联苯
反应条件
1: n-propyl-magnesium bromide With zirconocene dichloride in tetrahydrofuran T=0°C; 0.5 h; 2: With 2,4-dimethylpentan-3-one in tetrahydrofuran T=25°C; 3 h; 3: 3-methoxy-iodobenzene With triphenylphosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in tetrahydrofuran T=65°C; 3 h;
参考文献
Synlett, , # 11 art. no. Y00705ST, p. 1787 - 1788
→
反应条件
1115191-63-3
+
6161-50-8
3,3-二甲氧基联苯
反应条件
triethylamine in acetonitrile T=0 - 20°C; Inert atmosphere; Reagent/catalyst;
参考文献
Chemistry - A European Journal, , vol. 19, # 20 p. 6225 - 6229
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