2-(2-甲基苯氧基)乙醇合成路线 (共 14 条)
反应条件
pyridine; thionyl chloride; chloroform
参考文献
Givaudan and Cie.
Patent: DE887507 , 1949 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Givaudan Corp.
Patent: US2688638 , 1951 ;
Full Text Show Details
Gump; Nikawitz
Journal of the American Chemical Society, 1950 , vol. 72, p. 3846,3848, 3850
参考文献
Tetrahedron, , vol. 52, # 1 p. 177 - 184
参考文献
A. H. Robins Company, Incorporated
Patent: US5194446 A1, 1993 ;
反应条件
potassium carbonate; copper dichloride
T=130°C; 20 h; Inert atmosphereSchlenk technique;
参考文献
Liu, Yajun; Park, Se Kyung; Xiao, Yan; Chae, Junghyun
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 26 p. 4747 - 4753
参考文献
Givaudan and Cie.
Patent: DE887507 , 1949 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Givaudan Corp.
Patent: US2688638 , 1951 ;
反应条件
methanol; pyridinium p-toluenesulfonate
T=20°C; 16 h;
参考文献
Elhalem, Eleonora; Bailey, Brian N.; Docampo, Roberto; Ujvary, Istvan; Szajnman, Sergio H.; Rodriguez, Juan B.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 18 p. 3984 - 3999
反应条件
1.1: KOH / dimethylsulfoxide / 0.08 h / 20 °C
1.2: 85 percent / dimethylsulfoxide / 16 h / 20 °C
2.1: 41 percent / PPTs; MeOH / 16 h / 20 °C
View Scheme
参考文献
Elhalem, Eleonora; Bailey, Brian N.; Docampo, Roberto; Ujvary, Istvan; Szajnman, Sergio H.; Rodriguez, Juan B.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 18 p. 3984 - 3999
反应条件
ethanol; sodium ethanolate
T=70°C;
参考文献
Boyd; Marle
Journal of the Chemical Society, 1914 , vol. 105, p. 2123
参考文献
Halazy; Ehrhard; Eggenspiller; Berges-Gross; Danzin
Tetrahedron, 1996 , vol. 52, # 1 p. 177 - 184
反应条件
analoge Reaktion mit Propylenoxyd bei 70grad; Kinetics;
参考文献
Boyd; Marle
Journal of the Chemical Society, 1914 , vol. 105, p. 2123