in benzene addn. of 7 equiv. of phosphine to Pd(0) complex in benzene, 12 h; filtered, addn. of ether, crystn. after several days, identified by x-ray diffraction and 31P-NMR spectroscopy;
参考文献
Paul, Frederic; Patt, Joe; Hartwig, John F.
Journal of the American Chemical Society, 1994 , vol. 116, # 13 p. 5969 - 5970
sodium hydroxide in ethanol; toluene N2 atmosphere, addn. of EtOH soln. of NaOH to toluene suspension of Pd complex and phosphane ligand, 90°C (5 h), cooling; filtration, washing (water, EtOH and Et2O), drying (vacuum);
参考文献
Beller, Matthias; Riermeier, Thomas H.
European Journal of Inorganic Chemistry, 1998 , # 1 p. 29 - 35
Jacobi, Bridey Grant; Laitar, David S.; Pu, Lihung; Wargocki, Michael F.; DiPasquale, Antonio G.; Fortner, Kevin C.; Schuck, Stephany M.; Brown, Seth N.
Inorganic Chemistry, 2002 , vol. 41, # 18 p. 4815 - 4823
