2,7-二溴-9,10-二氢菲合成路线 (共 6 条)
反应条件
1: 23 percent / Ph3P, Et3N / PdCl2 / benzene / 4 h / 150 °C / 29736 Torr 2: 94 percent / aq. K2CO3 / methanol / 18 h / Heating View Scheme
参考文献
Abell, Andrew D.; Brandt, Martin; Levy, Mark A.; Holt, Dennis A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 11 p. 1663 - 1667
反应条件
chromium(VI) oxide; acetic acid in water T=20°C; Cooling with ice;
参考文献
Gautrot, Julien E.; Hodge, Philip; Helliwell, Madeleine; Raftery, James; Cupertino, Domenico
Journal of Materials Chemistry, 2009 , vol. 19, # 24 p. 4148 - 4156
反应条件
1: With N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 2: With potassium acetate; acetic acid in tetrachloromethane Heating; Further stages.;
参考文献
Tian, Hongkun; Shi, Jianwu; Dong, Shaoqiang; Yan, Donghang; Wang, Lixiang; Geng, Yanhou; Wang, Fosong
Chemical Communications, 2006 , # 33 p. 3498 - 3500
参考文献
Idemitsu Kosan Co., Ltd.
Patent: US2007/29927 A1, 2007 ;
反应条件
bromine; iron(III) chloride in chloroform
T=20°C;
参考文献
Tian, Hongkun; Shi, Jianwu; Dong, Shaoqiang; Yan, Donghang; Wang, Lixiang; Geng, Yanhou; Wang, Fosong
Chemical Communications, 2006 , # 33 p. 3498 - 3500
参考文献
Idemitsu Kosan Co., Ltd.
Patent: US2007/29927 A1, 2007 ;