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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
61653-33-6
合成路线
(共 12 条)
61653-33-6
→
反应条件
589-16-2
4-乙基苯胺
反应条件
perchloric acid in isopropyl alcohol; acetonitrile T=25°C; pH=2; 0.7 h; Inert atmosphereIrradiation;
参考文献
Farhadi, Saeid; Sepahvand, Shahnaz
Journal of Molecular Catalysis A: Chemical, 2010 , vol. 318, # 1-2 p. 75 - 84
589-16-2
4-乙基苯胺
→
反应条件
61653-33-6
反应条件
1,4-dibenzyl-1,4-diazoniabicyclo[2.2.2]octane chlorochromate in acetonitrile 0.25 h; Heating;
参考文献
xxx
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 2000 , vol. 39, # 11 p. 863 - 866
100-12-9
对乙基硝基苯
→
反应条件
61653-33-6
反应条件
bismuth; potassium hydroxide in methanol Reduction; Reductive coupling; 0.133333 h; Microwave irradiation;
参考文献
Laskar, Dhrubojyoti Dey; Prajapati, Dipak; Sandhu, Jagir S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 2000 , # 1 p. 67 - 70
23595-86-0
→
反应条件
61653-33-6
反应条件
iron bei der Destillation;
参考文献
Cline; Reid
Journal of the American Chemical Society, 1927 , vol. 49, p. 3155
28943-92-2
→
反应条件
61653-33-6
反应条件
oxygen in ethanol
参考文献
Newbold,B.T.; Tong,D.
Canadian Journal of Chemistry, 1964 , vol. 42, p. 836 - 842
22955-65-3
+
589-16-2
4-乙基苯胺
→
反应条件
61653-33-6
反应条件
in ethanol; acetic acid 1.) 10 deg C 2.) 55 deg C, 2 h;
参考文献
Dabrowski; Kenig; Raszewski; Kedzierski; Sadowska
Molecular crystals and liquid crystals, 1980 , vol. 61, # 1-2 p. 61 - 78
29743-18-8
p-甲氧基苄烯-p-乙基苯胺
→
反应条件
123-11-5
大茴香醛
+
61653-33-6
反应条件
water; benzhydroxamic acid chloride in methanol T=44.85°C; Oxidation; Kinetics;
参考文献
Mohamed Kassim; Basheer Ahamed
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 1999 , vol. 38, # 6 p. 533 - 540
67302-67-4
→
反应条件
100-52-7
苯甲醛
+
61653-33-6
反应条件
water; benzhydroxamic acid chloride in methanol T=44.85°C; Oxidation; Kinetics;
参考文献
Mohamed Kassim; Basheer Ahamed
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 1999 , vol. 38, # 6 p. 533 - 540
58761-10-7
→
反应条件
104-87-0
对甲基苯甲醛
+
61653-33-6
反应条件
water; benzhydroxamic acid chloride in methanol T=44.85°C; Oxidation; Kinetics;
参考文献
Mohamed Kassim; Basheer Ahamed
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 1999 , vol. 38, # 6 p. 533 - 540
67302-68-5
→
反应条件
104-88-1
4-氯苯甲醛
+
61653-33-6
反应条件
water; benzhydroxamic acid chloride in methanol T=44.85°C; Oxidation; Kinetics; Further Variations:reagents conc.;
参考文献
Mohamed Kassim; Basheer Ahamed
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 1999 , vol. 38, # 6 p. 533 - 540
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