反应条件
1: methyllithium With cerium(III) chloride in tetrahydrofuran; diethyl ether
T=-78°C; 0.583333 h; Inert atmosphere;
2: C18H27ClO2 in tetrahydrofuran; diethyl ether
T=-78 - 0°C; 1.78333 h; Inert atmosphere;
3: With hydrogenchloride in tetrahydrofuran; diethyl ether; water
T=0 - 23°C; Inert atmosphere;
参考文献
White, David E.; Stewart, Ian C.; Seashore-Ludlow, Brinton A.; Grubbs, Robert H.; Stoltz, Brian M.
Tetrahedron, 2010 , vol. 66, # 26 p. 4668 - 4686