反应条件
1: 3-Hexylthiophene With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-78°C; 2 h; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran; hexane 1 h; Overall yield = 90 percent; Overall yield = 610 mg; regioselective reaction;
参考文献
Seyler, Helga; Haid, Stefan; Kwon, Tae-Hyuk; Jones, David J.; Baeuerle, Peter; Holmes, Andrew B.; Wong, Wallace W. H.
Australian Journal of Chemistry, 2013 , vol. 66, # 2 p. 151 - 156
