(S)-(+)-2-辛醇合成路线 (共 200 条)
反应条件
in acetone 20 h; Ambient temperaturelipase PS, phosphate buffer; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 5 p. 557 - 562
反应条件
hydroxide; triphenylphosphine; diethylazodicarboxylate 1.) THF, - 30 deg C; ee(S) : 65percent; Multistep reaction. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 22, # 52 p. 5279 - 5282
反应条件
copper(l) iodide; magnesium 1.) THF, 1 h, 2.) THF, O deg C, 1 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 23, # 15 p. 2159 - 2169
反应条件
sodium; aluminum dichloride hydride 1.) ether, 0 deg C, 2 h; 2.) liquid ammonia; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 5 p. 334 - 335
参考文献
Journal of the Chemical Society, , p. 1236,1241
反应条件
porcine pancreatic lipase in hexane T=20°C; 120 h; var. solvents and reaction times; reaction with 1-phenylethanol; Product distribution;
参考文献
Acta chemica Scandinavica (Copenhagen, Denmark : 1989), , vol. 44, # 10 p. 1032 - 1035
反应条件
D-glucose; E. coli flavodoxin reductase; flavodoxin YkuN from Bacillus subtilis; glucose dehydrogenase from B. megaterium; P450 monooxygenase from Nocardia farcinica; NADP+; bovine serum albumin; catalase from bovine liver in ethanol T=25°C; 24 h; Enzymatic reaction; Catalytic behaviorKinetics; Reagent/catalystSolvent; stereoselective reaction;
参考文献
Chemical Communications, , vol. 50, # 31 p. 4089 - 4091
反应条件
D-glucose; minimal medea according to Dworkin et al T=30°C; Oxidation; 18 h; Microbiological reactionBacillus megaterium; Product distribution;
参考文献
European Journal of Organic Chemistry, , # 16 p. 2923 - 2926
反应条件
Title compound not separated from byproducts;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 37, # 6 p. 1653 - 1655
反应条件
ee = 78percent; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 24, # 42 p. 4581 - 4584