(S)-(+)-2-辛醇合成路线 （共 200 条）
反应条件
hydrogen; palladium on activated charcoal in methanol Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 26, # 28 p. 3369 - 3372
反应条件
(-)-sparteine in acetonitrile electrolysis: 'H' type divided cell separated by membrane Nafion 117, NaClO4 as supporting electrolyte, TEMPO-modified grafite felt electrode, charge passed 1.09 F mol-1, electrolysis potential 0.60 V (vs. Ag/AgCl);
参考文献
Chemical Communications, , # 24 p. 2745 - 2746
反应条件
(R)-2-(piperidin-1-yl)-1,1,2-triphenylethanol in hexane T=22°C; 36 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 15, # 13 p. 2085 - 2090
反应条件
1: 85 percent / AlH3 / diethyl ether 2: H2SO4 / methanol / 0.5 h / -10 - 0 °C 3: H2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4728 - 4731
反应条件
1: 90 percent / TBHP, VO(acac)2 2: 67 percent / H5IO6 / tetrahydrofuran; H2O 3: diethyl ether / -78 - 0 °C 4: 85 percent / AlH3 / diethyl ether 5: H2SO4 / methanol / 0.5 h / -10 - 0 °C 6: H2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4728 - 4731
反应条件
1: 80 percent / CrO3, pyridine 2: diethyl ether / -78 - 0 °C 3: 85 percent / AlH3 / diethyl ether 4: H2SO4 / methanol / 0.5 h / -10 - 0 °C 5: H2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4728 - 4731
反应条件
1: 91 percent / Ti(Oi-Pr)4, L(+)DET 2: 80 percent / CrO3, pyridine 3: diethyl ether / -78 - 0 °C 4: 85 percent / AlH3 / diethyl ether 5: H2SO4 / methanol / 0.5 h / -10 - 0 °C 6: H2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4728 - 4731
反应条件
1: diethyl ether / -78 - 0 °C 2: 85 percent / AlH3 / diethyl ether 3: H2SO4 / methanol / 0.5 h / -10 - 0 °C 4: H2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4728 - 4731
反应条件
1: 67 percent / H5IO6 / tetrahydrofuran; H2O 2: diethyl ether / -78 - 0 °C 3: 85 percent / AlH3 / diethyl ether 4: H2SO4 / methanol / 0.5 h / -10 - 0 °C 5: H2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 24 p. 4728 - 4731
反应条件
1: methyl iodide; diethyl ether / Erhitzen der aus der erhaltenen quartaeren Ammoniumjodid hergestellten wss. Ammoniumhydroxid-Loesung 2: lithium alanate; diethyl ether View Scheme
参考文献
Journal of the American Chemical Society, , vol. 80, p. 1611
