in pyridine-D5
T=40 - 50°C; 12 h; Irradiation; Title compound not separated from byproducts;
参考文献
Borisova, I. V.; Zemlyanskii, N. N.; Khrustalev, V. N.; Nechaev, M. S.; Kuznetsova, M. G.; Ustynyuk, Yu. A.
Russian Chemical Bulletin, 2002 , vol. 51, # 4 p. 678 - 683
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2002 , # 4 p. 627 - 631
in neat (no solvent)
from As mirror with C2H5 radical (thermal decompn. of tetraethyl lead at low pressure in H2 stream);; pptn. on cooling with liquid air; fractionated distn.;;
参考文献
Paneth, F.
Transactions of the Faraday Society, 1934 , vol. 30, p. 179
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Gmelin Handbook: As: MVol., 52, page 184 - 186
in diethyl ether
1 h; Title compound not separated from byproducts;
参考文献
Borisova, I. V.; Zemlyanskii, N. N.; Khrustalev, V. N.; Nechaev, M. S.; Kuznetsova, M. G.; Ustynyuk, Yu. A.
Russian Chemical Bulletin, 2002 , vol. 51, # 4 p. 678 - 683
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2002 , # 4 p. 627 - 631
