carbon tetrabromide; triphenylphosphine in benzene
T=60°C; Yield given. Yields of byproduct given;
参考文献
MacCorquodale, Finlay; Walton, John C.; Hughes, Lise; Ingold, Keith U.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 1893 - 1900
1: 73 percent / NaOH / ethanol / 1 h / Heating
2: 35 percent / pyridine / 1 h / Heating
3: 2.91 g / LiAlH4 / diethyl ether / 3 h / Heating
4: CBr4, PPh3 / benzene / 60 °C
View Scheme
参考文献
MacCorquodale, Finlay; Walton, John C.; Hughes, Lise; Ingold, Keith U.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 1893 - 1900
1: 35 percent / pyridine / 1 h / Heating
2: 2.91 g / LiAlH4 / diethyl ether / 3 h / Heating
3: CBr4, PPh3 / benzene / 60 °C
View Scheme
参考文献
MacCorquodale, Finlay; Walton, John C.; Hughes, Lise; Ingold, Keith U.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 1893 - 1900
1: 2.91 g / LiAlH4 / diethyl ether / 3 h / Heating
2: CBr4, PPh3 / benzene / 60 °C
View Scheme
参考文献
MacCorquodale, Finlay; Walton, John C.; Hughes, Lise; Ingold, Keith U.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 1893 - 1900
