5-氯甲基-5-碘甲基-1,3-二恶烷合成路线 （共 3 条）
反应条件
sulfuric acid in 1,4-dioxane
5 h; Heating;
参考文献
Kurmaeva, E. S.; Chalova, O. B.; Chistoedova, G. P.; Lapuka, L. F.; Kiladze, T. K.; et al.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 1 p. 119 - 123
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 1 p. 131 - 135
反应条件
sodium iodide in acetone
T=62°C; 175 h;
参考文献
Kurmaeva, E. S.; Chalova, O. B.; Chistoedova, G. P.; Lapuka, L. F.; Kiladze, T. K.; et al.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 1 p. 119 - 123
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 1 p. 131 - 135
反应条件
1: conc. H2SO4 / dioxane / 5 h / Heating
2: 22 percent / NaI / acetone / 175 h / 62 °C
View Scheme
参考文献
Kurmaeva, E. S.; Chalova, O. B.; Chistoedova, G. P.; Lapuka, L. F.; Kiladze, T. K.; et al.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 1 p. 119 - 123
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 1 p. 131 - 135
