反应条件
1: N-methyl-N-phenylmethanesulfonamide With zinc(II) chloride; lithium hexamethyldisilazane in tetrahydrofuran
T=-20 - 20°C; 1 h; Inert atmosphere;
2: bromobenzene With palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran
T=20 - 65°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Zhou, Gang; Ting, Pauline; Aslanian, Robert; Piwinski, John J.
Organic Letters, 2008 , vol. 10, # 12 p. 2517 - 2520