反应条件
sodium hydroxide; dihydrogen peroxide; (-)-β-methallyldiisopinocampheylborane
1.) anhydrous ethyl ether, -78 deg C, 1 h, 25 deg C, 1 h. 2.) -78 deg C, 1 h, 30 deg C, 3 h.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Jadhav, Prabhakar K.; Perumal, P. Thirumalai
Tetrahedron Letters, 1984 , vol. 25, # 45 p. 5111 - 5114