1: oxalyl dichloride / 1 h / 50 °C / Inert atmosphere
2: dichloromethane / 20 °C / Inert atmosphere; Cooling with ice
View Scheme
参考文献
Vaillard, Victoria A.; Guastavino, Javier F.; Buden, Maria E.; Bardagi, Javier I.; Barolo, Silvia M.; Rossi, Roberto A.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1507 - 1519
in dichloromethane
T=20°C; Inert atmosphereCooling with ice;
参考文献
Vaillard, Victoria A.; Guastavino, Javier F.; Buden, Maria E.; Bardagi, Javier I.; Barolo, Silvia M.; Rossi, Roberto A.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1507 - 1519
