反应条件
1: 1) NaH / 1) THF, room temperature, 1 h, 2) -78 deg C -> room temperature, 2 h
2: 1) NaH, 2) n-BuLi / 1) hexane, THF, room temperature, 30 min., 2) a) -78 deg C, 1 h, b) up to room temperature, 1 h
View Scheme
参考文献
Hermann, Christine K. F.; Campbell, James A.; Greenwood, Thomas D.; Lewis, Judith A.; Wolfe, James F.
Journal of Organic Chemistry, 1992 , vol. 57, # 20 p. 5328 - 5334
