反应条件
1: 1.) triethylamine, 2.) NaClO4 / 1.) DMF, from 130 to 140 ,degC, 45 min, 2.) H2O, from 0 to 5 deg C, 1 d
2: 91 percent / conc. HBr / Heating
View Scheme
参考文献
Neiland, O. Ya.; Kraupsha, I. L.; Gudele, I. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993 , vol. 29, # 12 p. 1428 - 1434
Khimiya Geterotsiklicheskikh Soedinenii, 1993 , # 12 p. 1653 - 1661