in neat (no solvent) 2 equiv of Sn deriv. and 1 equiv of the cycloalkene heating at 180°C for 64 h under Ar; isolated by gas chromy. at 230°C; identified by NMR and mass spectra;
参考文献
Quintard, Jean-Paul; Degueil-Castaing, Marie; Barbe, Bernard; Petraud, Michel
Journal of Organometallic Chemistry, 1982 , vol. 234, # 1 p. 41 - 62
in not given byproducts: anti-7-deuterionorbonene; reaction mechanism discussed;;
参考文献
Warkentin; Sanford
Journal of the American Chemical Society, 1968 , vol. 90, p. 1667
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.2, page 52 - 57
in not given byproducts: anti-7-deuterionorbonene; reaction mechanism discussed;;
参考文献
Warkentin; Sanford
Journal of the American Chemical Society, 1968 , vol. 90, p. 1667
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.2, page 52 - 57
Green, F. D.; Lowry, H. N.
Journal of Organic Chemistry, 1967 , vol. 32, p. 882 - 885
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.2, page 52 - 57
Pommier, J. C.; Chevolleau, D.
Journal of Organometallic Chemistry, 1974 , vol. 74, p. 405 - 416
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.2, page 52 - 57
acetylene in methanol byproducts: olefine; reaction at 150-155°C;;
参考文献
Pereyre, M.; Quintard, J. P.; Godet, J. Y.; Valade, J.
Organometal. Chem. Syn., 1971 , vol. 1, p. 269 - 288
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5.4.5, page 60 - 61
