(3,5-双(三氟甲基)苯乙炔基)三甲基硅烷合成路线 (共 3 条)
反应条件
sodium hydroxide in tetrahydrofuran; methanol; water 1 h; Inert atmosphere;
参考文献
Mujkic, Monika; Lentz, Dieter
Dalton Transactions, 2012 , vol. 41, # 3 p. 839 - 849
反应条件
piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
12 h;
参考文献
Wilson, James N.; Josowicz, Mira; Wang, Yiqing; Bunz, Uwe H. F.
Chemical Communications, 2003 , # 24 p. 2962 - 2963
反应条件
copper(l) iodide; palladium diacetate; diethylamine; triphenylphosphine in toluene
Sonogashira Cross-Coupling; 0.166667 h; Schlenk technique;
参考文献
Gallego, Daniel; Brueck, Andreas; Irran, Elisabeth; Meier, Florian; Kaupp, Martin; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 41 p. 15617 - 15626