1-(4-氯苯基)-2-[(4-甲基苯基)磺酰基]乙酮合成路线 （共 19 条）
反应条件
1: 42 percent / Et3N / dimethylformamide / 48 h / Heating
2: 75 percent / <RuCl2(PPh3)3> / benzene / 7 h / 120 °C
View Scheme
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 783 - 786
反应条件
1: iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide; acetonitrile / 0.5 h / 20 °C
2: dimethyl sulfoxide; acetonitrile / 1 h / 20 °C
View Scheme
参考文献
Samakkanad, Natthapol; Katrun, Praewpan; Techajaroonjit, Thanachart; Hlekhlai, Sornsiri; Pohmakotr, Manat; Reutrakul, Vichai; Jaipetch, Thaworn; Soorukram, Darunee; Kuhakarn, Chutima
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-N0148-OP, p. 1693 - 1699
反应条件
1: potassium hydroxide / ethanol / 1 h / 20 °C
2: toluene-4-sulfonic acid / benzene / |Dean-Stark
3: dihydrogen peroxide / acetic acid / |Heating
View Scheme
参考文献
Savka; Pohodylo; Obushak
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 296 - 297
Zhurnal Organicheskoi Khimii, 2014 , vol. 50, # 2 p. 303 - 304,2
反应条件
1: toluene-4-sulfonic acid / benzene / |Dean-Stark
2: dihydrogen peroxide / acetic acid / |Heating
View Scheme
参考文献
Savka; Pohodylo; Obushak
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 296 - 297
Zhurnal Organicheskoi Khimii, 2014 , vol. 50, # 2 p. 303 - 304,2
反应条件
1: potassium hydroxide / ethanol / 1 h / 20 °C
2: toluene-4-sulfonic acid / benzene / |Dean-Stark
3: dihydrogen peroxide / acetic acid / |Heating
View Scheme
参考文献
Savka; Pohodylo; Obushak
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 296 - 297
Zhurnal Organicheskoi Khimii, 2014 , vol. 50, # 2 p. 303 - 304,2
反应条件
in dimethyl sulfoxide; acetonitrile
T=20°C; 1 h;
参考文献
Samakkanad, Natthapol; Katrun, Praewpan; Techajaroonjit, Thanachart; Hlekhlai, Sornsiri; Pohmakotr, Manat; Reutrakul, Vichai; Jaipetch, Thaworn; Soorukram, Darunee; Kuhakarn, Chutima
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-N0148-OP, p. 1693 - 1699
反应条件
1: acetone / 48 h / 30 °C
2: 4 h / 30 °C / Ionic liquid
View Scheme
参考文献
Kumar, Anil; Muthyala, Manoj Kumar
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5368 - 5370
反应条件
1: TsN3, Et3N / ethanol
2: aq. HClO4, Cu
View Scheme
参考文献
Ferdinand,G. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 1713 - 1726
反应条件
1: 80 percent / iodine monochloride / acetic acid / 14 h / 20 °C
2: 89 percent / aq. NaOH / 0.5 h / 20 °C
View Scheme
参考文献
Suryakiran; Srikanth Reddy; Suresh; Lakshman; Venkateswarlu
Tetrahedron Letters, 2006 , vol. 47, # 26 p. 4319 - 4323
