4-甲基-2(对甲苯磺酰基)苯乙酮合成路线 （共 21 条）
反应条件
in neat (no solvent)
T=30°C; 4 h;
参考文献
Muthyala, Manoj Kumar; Choudhary, Sunita; Kumar, Anil
RSC Advances, 2014 , vol. 4, # 27 p. 14297 - 14303
反应条件
1: 67 percent / Et3N / dimethylformamide / 48 h / Heating
2: 70 percent / <RuCl2(PPh3)3> / benzene / 7 h / 120 °C
View Scheme
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 783 - 786
反应条件
dihydrogen peroxide; acetic acid
参考文献
Shingare; Siddiqui
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 2 p. 154 - 158
反应条件
1: AIBN / benzene
2: 83 percent / TFA / tetrahydrofuran / Heating
View Scheme
参考文献
Qian, Hao; Huang, Xian
Synthesis, 2006 , # 12 p. 1934 - 1936
反应条件
1: iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide; acetonitrile / 0.5 h / 20 °C
2: dimethyl sulfoxide; acetonitrile / 1 h / 20 °C
View Scheme
参考文献
Samakkanad, Natthapol; Katrun, Praewpan; Techajaroonjit, Thanachart; Hlekhlai, Sornsiri; Pohmakotr, Manat; Reutrakul, Vichai; Jaipetch, Thaworn; Soorukram, Darunee; Kuhakarn, Chutima
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-N0148-OP, p. 1693 - 1699
反应条件
1: potassium hydroxide / ethanol / 1 h / 20 °C
2: toluene-4-sulfonic acid / benzene / |Dean-Stark
3: dihydrogen peroxide / acetic acid / |Heating
View Scheme
参考文献
Savka; Pohodylo; Obushak
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 296 - 297
Zhurnal Organicheskoi Khimii, 2014 , vol. 50, # 2 p. 303 - 304,2
反应条件
1: potassium hydroxide / ethanol / 1 h / 20 °C
2: toluene-4-sulfonic acid / benzene / |Dean-Stark
3: dihydrogen peroxide / acetic acid / |Heating
View Scheme
参考文献
Savka; Pohodylo; Obushak
Russian Journal of Organic Chemistry, 2014 , vol. 50, # 2 p. 296 - 297
Zhurnal Organicheskoi Khimii, 2014 , vol. 50, # 2 p. 303 - 304,2
反应条件
in dimethyl sulfoxide; acetonitrile
T=20°C; 1 h;
参考文献
Samakkanad, Natthapol; Katrun, Praewpan; Techajaroonjit, Thanachart; Hlekhlai, Sornsiri; Pohmakotr, Manat; Reutrakul, Vichai; Jaipetch, Thaworn; Soorukram, Darunee; Kuhakarn, Chutima
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-N0148-OP, p. 1693 - 1699
反应条件
2: 30percent H2O2, acetic acid
View Scheme
参考文献
Shingare; Siddiqui
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 2 p. 154 - 158
反应条件
2: 30percent H2O2, acetic acid
View Scheme
参考文献
Shingare; Siddiqui
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 2 p. 154 - 158
