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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
61822-18-2
合成路线
（共 14 条）
92248-06-1
双(3-甲氧基苯基)胺
→
反应条件
61822-18-2
反应条件
copper diacetate; palladium diacetate in N,N-dimethyl-formamide T=130°C; 1.16667 h; Inert atmosphereMicrowave irradiation;
参考文献
Bautista, Rafael; Montoya, Pablo A.; Rebollar, Araceli; Burgueno, Eleuterio; Tamariz, Joaquin
Molecules, 2013 , vol. 18, # 9 p. 10334 - 10351
13606-06-9
→
反应条件
61822-18-2
反应条件
triethyl phosphite T=160°C; 16 h; Inert atmosphere;
参考文献
Kamino, Brett A.; Mills, Bridget; Reali, Christopher; Gretton, Michael J.; Brook, Michael A.; Bender, Timothy P.
Journal of Organic Chemistry, 2012 , vol. 77, # 4 p. 1663 - 1674
1424799-10-9
→
反应条件
61822-18-2
反应条件
1: With potassium tert-butylate; oxygen in tetrahydrofuran; dimethyl sulfoxide T=20°C; P=760.051 Torr; 26 h; 2: With water in tetrahydrofuran; dimethyl sulfoxide
参考文献
Qiu, Youai; Ma, Dengke; Fu, Chunling; Ma, Shengming
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1666 - 1671
67-56-1
甲醇
+
124-41-4
甲醇钠
+
136630-39-2
2,7-二溴咔唑
→
反应条件
61822-18-2
反应条件
copper(l) iodide in N,N-dimethyl-formamide T=110°C; 20 h; Inert atmosphereSealed tube;
参考文献
Louillat, Marie-Laure; Patureau, Frederic W.
Organic Letters, 2013 , vol. 15, # 1 p. 164 - 167
124-41-4
甲醇钠
+
136630-39-2
2,7-二溴咔唑
→
反应条件
61822-18-2
反应条件
copper(l) iodide in methanol; N,N-dimethyl-formamide T=110°C; 20 h; Schlenk techniqueInert atmosphere;
参考文献
Louillat, Marie-Laure; Biafora, Agostino; Legros, Fabien; Patureau, Frederic W.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3505 - 3509
Angew. Chem., 2014 , vol. 53, # 13 p. 3573 - 3577,5
96-96-8
4-甲氧基-2-硝基苯胺
→
反应条件
61822-18-2
反应条件
1.1: hydrogen bromide; sodium nitrite / water / 2 h / 20 °C 1.2: 0.08 h / 80 °C / Inert atmosphere 2.1: copper / 180 - 210 °C 3.1: triethyl phosphite / 4 h / 170 °C / Inert atmosphere View Scheme
参考文献
Tsuchiya, Kousuke; Sakaguchi, Kota; Kasuga, Hidemasa; Kawakami, Akira; Taka, Hideo; Kita, Hiroshi; Ogino, Kenji
Polymer, 2010 , vol. 51, # 3 p. 616 - 622
1424799-08-5
→
反应条件
61822-18-2
反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -40 °C / |Inert atmosphere 1.2: 1.25 h / -40 - 20 °C / |Inert atmosphere 2.1: gold(I) chloride / toluene / 11.5 h / 20 °C / |Schlenk technique; |Inert atmosphere 3.1: potassium tert-butylate; oxygen / tetrahydrofuran; dimethyl sulfoxide / 26 h / 20 °C / 760.05 Torr View Scheme
参考文献
Qiu, Youai; Ma, Dengke; Fu, Chunling; Ma, Shengming
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1666 - 1671
1424799-09-6
→
反应条件
61822-18-2
反应条件
1: gold(I) chloride / toluene / 11.5 h / 20 °C / |Schlenk technique; |Inert atmosphere 2: potassium tert-butylate; oxygen / tetrahydrofuran; dimethyl sulfoxide / 26 h / 20 °C / 760.05 Torr View Scheme
参考文献
Qiu, Youai; Ma, Dengke; Fu, Chunling; Ma, Shengming
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1666 - 1671
5344-78-5
4-溴-3-硝基苯甲醚
→
反应条件
61822-18-2
反应条件
1: copper / 180 - 210 °C 2: triethyl phosphite / 4 h / 170 °C / Inert atmosphere View Scheme
参考文献
Tsuchiya, Kousuke; Sakaguchi, Kota; Kasuga, Hidemasa; Kawakami, Akira; Taka, Hideo; Kita, Hiroshi; Ogino, Kenji
Polymer, 2010 , vol. 51, # 3 p. 616 - 622
536-90-3
间氨基苯甲醚
→
反应条件
61822-18-2
反应条件
1: toluene / 12 h / |Inert atmosphere; |Dean-Stark; |Reflux 2: palladium 10 on activated carbon; methanol / 48 h / 210 °C / |Inert atmosphere 3: potassium carbonate / acetone / 12 h / |Inert atmosphere; |Reflux 4: palladium diacetate; copper diacetate / N,N-dimethyl-formamide / 1.17 h / 130 °C / |Inert atmosphere; |Microwave irradiation View Scheme
参考文献
Bautista, Rafael; Montoya, Pablo A.; Rebollar, Araceli; Burgueno, Eleuterio; Tamariz, Joaquin
Molecules, 2013 , vol. 18, # 9 p. 10334 - 10351
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