2-(2-苯基乙基)色原酮合成路线 （共 4 条）
反应条件
hydrogenchloride in acetic acid
T=120°C; 0.75 h;
参考文献
Williams, Dwight A.; Smith, Cameron; Zhang, Yan
Tetrahedron Letters, 2013 , vol. 54, # 32 p. 4292 - 4295
反应条件
ammonium formate; palladium on activated charcoal in methanol
1 h; Heating;
参考文献
Goel, Sharda; Shashi; Makrandi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 2 p. 535 - 536
反应条件
1: sodium hydride / tetrahydrofuran; mineral oil / |Inert atmosphere; |Reflux
2: hydrogenchloride / methanol / 14 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Zhao, Dongbing; Beiring, Bernhard; Glorius, Frank
Angewandte Chemie - International Edition, 2013 , vol. 52, # 32 p. 8454 - 8458
Angew. Chem., 2013 , vol. 125, # 32 p. 8612 - 8616,5
反应条件
1.1: sodium hydride / tetrahydrofuran / 1.17 h / |Reflux
1.2: 24.25 h / 20 °C
2.1: hydrogenchloride / acetic acid / 0.75 h / 120 °C
View Scheme
参考文献
Williams, Dwight A.; Smith, Cameron; Zhang, Yan
Tetrahedron Letters, 2013 , vol. 54, # 32 p. 4292 - 4295
